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Record W2331847931 · doi:10.15278/isms.2015.tb04

FAR-INFRARED SYNCHROTRON-BASED SPECTROSCOPY OF PROTON TUNNELLING IN MALONALDEHYDE

2015· article· en· W2331847931 on OpenAlexaffabout
E. Scott Goudreau, Stephen T. Ross, D. W. Tokaryk

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldChemistry
TopicMolecular Spectroscopy and Structure
Canadian institutionsUniversity of New Brunswick
Fundersnot available
KeywordsQuantum tunnellingExcited stateGround stateSpectroscopyInfraredChemistryAtomic physicsMaterials sciencePhysicsOpticsOptoelectronics

Abstract

fetched live from OpenAlex

Malonaldehyde (C 3 O 2 H 4 ) is a prototype molecule for the study of intramolecular tunnelling proton transfer.In the case of malonaldehyde, this transfer occurs between the two terminal oxygen atoms in its open-ring structure.Although the ground state tunnelling splitting of 21 cm -1 has been accurately determined from microwave studies a , the splitting has never been obtained with high resolution in any excited vibrational state.The ν 6 vibrational band was investigated in a diode laser jet experiment b in 2004, but the researchers were not able to identify the (-) parity tunnelling component and so could not determine the splitting.We have collected high-resolution far-IR Fourier transform spectra from a number of fundamental vibrational bands of malonaldehyde at the CLS (Canadian Light Source) synchrotron in Saskatoon, Saskatchewan, exploiting the considerable gain in signal-to-noise ratio at the highest resolution available afforded by the intense and well-collimated beam.We will report on our tunnelling-rotation analysis of the anti-symmetric out-of-plane bend near 384 cm -1 and present its tunnelling splitting value.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.256
Teacher spread0.243 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2015
Admission routes2
Has abstractyes

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