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Record W2334246198 · doi:10.1021/ic302569c

A Theoretical Analysis of Supported Quintuple and Quadruple Chromium–Chromium Bonds

2013· article· en· W2334246198 on OpenAlexafffund
Sylvester Ndambuki, Tom Ziegler

Bibliographic record

VenueInorganic Chemistry · 2013
Typearticle
Languageen
FieldChemistry
TopicOrganometallic Complex Synthesis and Catalysis
Canadian institutionsUniversity of Calgary
FundersCanada Research ChairsWestern Canada Research Grid
KeywordsChemistryChromiumMetalTransition metalCrystallographyNatural bond orbitalValence (chemistry)Computational chemistryBond strengthBond energyChemical bondDensity functional theoryMoleculeCatalysisOrganic chemistry

Abstract

fetched live from OpenAlex

The extended transition state (ETS) energy decomposition scheme has been combined with the natural orbitals for chemical valence (NOCV) density decomposition method (ETS-NOCV) in a study on the shortest, fully supported metal-metal bond (Cr-Cr = 1.73 Å) in Cr2[Ar'NC(NMe2)NAr']2 [Ar' = C6H3-2,6(C6H3-2,6-Pr(i)2)2]. The scope of the ETS-NOCV method is further demonstrated by a metal-metal bond analysis of the paddlewheel M2(O2CCH3)4 (M = Cr, Mo, W) complexes. The influence of axial ligands as well as R' goups on the bridging ligands is also analyzed. In addition to the quintuple bonding components (σ(2), π(4), δ(4)) for Cr2[Ar'NC(NMe2)NAr']2 and quadruple components (σ(2), π(4), δ(2)) for the paddlewheel complexes, we notice additional stability (17-27 kcal/mol) introduced to the metal-metal bond from participation of the lone pairs residing on the π-systems of the bridging X-C-X (X = N, O) ligand. This is to our knowledge the first time that the strength of the metal-metal bonding components has been determined in a supported metal-metal bond by an energy decomposition scheme.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.449
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.4490.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.202
Teacher spread0.197 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations36
Published2013
Admission routes2
Has abstractyes

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