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Record W2334265164 · doi:10.1021/ie300596x

Physical and Chemical Mechanism for Increased Surface Area and Pore Volume of CaO in Water Hydration

2012· article· en· W2334265164 on OpenAlexfundno aff
Zhenchao Sun, Hao Chi, Liang‐Shih Fan

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2012
Typearticle
Languageen
FieldEngineering
TopicMetallurgical Processes and Thermodynamics
Canadian institutionsnot available
FundersGraymont
KeywordsVolume (thermodynamics)PorosityChemistryChemical engineeringWater of crystallizationDehydrationSpecific surface areaMoistureSolvation shellPrecipitationParticle (ecology)MineralogyMoleculeThermodynamicsOrganic chemistrySolvationCatalysis

Abstract

fetched live from OpenAlex

The present work explores the fundamental mechanism behind the increased surface area and pore volume of CaO after hydration. First, a widely believed mechanism, the “physical attrition theory”, is experimentally examined and is found to have limitations in explaining this phenomenon. Next, to explain the improvement of morphological properties by hydration, a typical water hydration process is examined by dividing the process into four independent chemical and physical substeps. The morphological changes of Ca(OH) 2 and its derived CaO by each substep are measured by Brunauer–Emmett–Teller (BET) analysis. During the first step, the intrinsic chemical conversion from CaO to Ca(OH) 2, the formed Ca(OH) 2 product layer disintegrates because of its low tensile strength and weak crack resistance, which explains the increases in surface area and pore volume by steam/moisture hydration as well as the rapid heat release during hydration. The physical interaction with water (the second step) slightly decreases the surface area and pore volume, possibly by lodging microparticles into the porous structure of bigger particles and inducing stronger particle agglomeration. The Ca(OH) 2 solid can further chemically bond water molecules (the third step), which significantly enlarges the solid volume during water-bonding and consequently generates a more porous structure during dehydration. The final precipitation of the dissolved Ca(OH) 2 (the fourth step) decreases the solid’s surface area and pore volume. This decrease is attributed to the formed microparticles from solution, which can plug some surface pores on the larger particles during the drying process.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.420
Threshold uncertainty score0.465

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.046
GPT teacher head0.276
Teacher spread0.230 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations24
Published2012
Admission routes1
Has abstractyes

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