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Record W2341886237 · doi:10.1021/acs.iecr.5b03996

Stripping Uranium from Seawater-Loaded Sorbents with the Ionic Liquid Hydroxylammonium Acetate in Acetic Acid for Efficient Reuse

2015· article· en· W2341886237 on OpenAlexaff
Paula Bertón, Steven P. Kelley, Robin D. Rogers

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2015
Typearticle
Languageen
FieldChemistry
TopicRadioactive element chemistry and processing
Canadian institutionsMcGill University
FundersOffice of Nuclear EnergySmall Business Innovation ResearchNuclear Energy University ProgramU.S. Department of Energy
KeywordsAcetic acidSeawaterChemistryUraniumReuseStripping (fiber)Ionic liquidInorganic chemistryNuclear chemistryOrganic chemistryMaterials scienceWaste managementMetallurgyCatalysis

Abstract

fetched live from OpenAlex

A new stripping and recovery process was developed to harvest the uranium recovered from seawater with amidoxime-functionalized polyethylene fiber sorbents and allow reuse of the sorbent without loss of capacity and without the need to recondition the sorbent before reuse. Hydroxylammonium acetate ([NH 3 OH][OAc])/aqueous acetic acid (AcOH) solutions were used as weakly acidic stripping agents and the stripped uranium as a soluble acetate was further immobilized on shrimp shells. These solutions also stripped the vanadium and other metal ions coadsorbed, which reduce capacity through competition with uranium for sorbent binding and can resist stripping even by strong acids. [NH 3 OH][OAc]/AcOH was found to allow recovery of more than 85% of the uranium although at a substantially longer time than the current 0.5 M HCl-stripping solutions, (less than 12 h vs 48–72 h, respectively); however, the use of HCl severely compromises the capacity of the sorbent in subsequent reuse (a 50% lost was observed on the third reuse of the fiber). Both [NH 3 OH][OAc] and the acetic acid were necessary to achieve high uranium recovery without sacrificing the sorbent’s capacity on reuse. The ability to reuse the sorbent without pretreatment and with minimal capacity loss could be an important step toward making the extraction of uranium from seawater energy-efficient and economically viable.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.028
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.002
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.102
GPT teacher head0.317
Teacher spread0.215 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2015
Admission routes1
Has abstractyes

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