Synthesis of Titania-Pillared Layered Niobic Acid with a High Specific Surface Area by using Sol-I ntercalation Method
Bibliographic record
Abstract
Hydrated titanium sol particles-in tercalated layered niobate was prep ared through the reaction between n-decylamine-intercalated niobate and hydrated product of tetrabutyl t itanate.The titania-pillared layered niobic acid then obtained by calcining the t itanium sol particles-intercalate d niobate at 450℃in air.The resultin g material has been characterized by means of XRD,IR,BET surface area and pore size d istribution measurement techniques.The pillared sample was porous(mainly mesopores),with a high BET surface area of 131.3m 2 ·g -1 and an in-terlayer distance of 1.26nm at 450℃.Test of thermal stability revealed t hat the structure of the titania-pillared layered niobic acid was stable after this material calcined at 550℃for 2h in air.
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How this classification was reachedexpand
Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.001 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.001 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.001 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one teacher head, not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".