Determination of Bifenthrin in Tea by Ultra Performance Convergence Chromatography and Gas Chromatography-Mass Spectrometry
Bibliographic record
Abstract
A method was developed for the determination of bifenthrin in tea by ultra performance convergence chromatography( UPC2). The samples were extracted with petroleum ether and cleaned up with Waters SepPakCarbon NH2,and then detected by UPC2. The mobile phase was the mixture of supercritical CO2 and acetonitrile at a flow rate of 1. 5 m L / min. The separation was conducted on a column of ACQUITY UPC2 TM BEH( 100 mm × 3. 0 mm,1. 7 μm). The UV detector was set at a wavelength of 220 nm. The detection limit was 20 μg / L. The linear range of bifenthrin was 0. 32- 10. 30 mg / L. The recoveries ranged from 88. 7% to98. 2%. The relative standard deviations( RSD) were from 1. 4% to 2. 8%. The result showed that the UPC2 was more efficient,rapid and low-cost than GC-MS. The method can meet the testing requirements of bifenthrin in tea. The efficacy of UPC2 on testing the concentration of bifenthrin in tea was compared with GC-MS based on National Proficiency Testing and the results were satisfactory.
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How this classification was reachedexpand
Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.001 | 0.001 |
| Meta-epidemiology (narrow) | 0.001 | 0.000 |
| Meta-epidemiology (broad) | 0.001 | 0.001 |
| Bibliometrics | 0.000 | 0.002 |
| Science and technology studies | 0.000 | 0.001 |
| Scholarly communication | 0.000 | 0.001 |
| Open science | 0.001 | 0.000 |
| Research integrity | 0.000 | 0.001 |
| Insufficient payload (model declined to judge) | 0.001 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one teacher head, not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".