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Record W2393502792

Studies on the Dilution Refolding and Aggregation Interaction of Bovine Carbonic Anhydrase B Induced by Urea

2010· article· en· W2393502792 on OpenAlexaff
Shixiang Wang

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicEnzyme function and inhibition
Canadian institutionsScience North
Fundersnot available
KeywordsChemistryUreaCarbonic anhydraseDilutionChromatographySize-exclusion chromatographyDissociation (chemistry)EnzymeOrganic chemistry
DOInot available

Abstract

fetched live from OpenAlex

The dilution refolding and aggregation interaction of bovine carbonic anhydrase B induced by urea were studied by using non-denatured PAGE,SDS-PAGE,size-exclusion chromatography and laser light-scattering. When the final urea concentration in renaturation solutions was higher than 2.0 mol/L,bovine carbonic anhydrase B existed in the renaturation solutions in unimolecular form and bi-molecular aggregate; when the final urea concentration was in the range of 1.0-2.0 mol/L,they existed in a unimolecular form,bi-molecular aggregate and a small amount of multi-molecular aggregate; and when the final urea concentration was lower or equal to 1.0 mol/L,a transparent supernatant and an opaque precipitate were separately formed in the dilution refolding of urea-induced bovine carbonic anhydrase B,a dynamic dissociation equilibrium existed in the bovine carbonic anhydrase B included in the supernatant and that included in the precipitate and in both the supernatant and precipitate,and bovine carbonic anhydrase B existed in a unimolecular form,bi-molecular and a small amount of multi-molecular aggregate. The bi-molecular and multi-molecular aggregates were formed through the hydrophobic and electrostatic interactions between the unimolecular bovine carbonic anhydrase B,and only if the concentrations of these components in renaturation solution were higher than a certain value and the urea concentration in the final renaturation solution was lower than a certain value,an aggregate precipitate could be formed through the non-covalent interactions among these components.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.278
Teacher spread0.259 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2010
Admission routes1
Has abstractyes

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