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Record W2477720359 · doi:10.1111/ggr.12131

Calcium Isotopic Compositions of Sixteen <scp>USGS</scp> Reference Materials

2016· article· en· W2477720359 on OpenAlexaff
Lanping Feng, Lian Zhou, Lu Yang, Donald J. DePaolo, Shuoyun Tong, Yongsheng Liu, T.L. Owens, Shan Gao

Bibliographic record

VenueGeostandards and Geoanalytical Research · 2016
Typearticle
Languageen
FieldEnvironmental Science
TopicIsotope Analysis in Ecology
Canadian institutionsNational Research Council Canada
FundersU.S. Geological SurveyState Key Laboratory of Geological Processes and Mineral ResourcesMinistry of Education of the People's Republic of ChinaNational Natural Science Foundation of China
KeywordsMineralogyCalciteNISTMass spectrometryGeologySeawaterIsotopeChemistryAnalytical Chemistry (journal)GeochemistryEnvironmental chemistryChromatography

Abstract

fetched live from OpenAlex

Calcium isotopic compositions of sixteen Ca‐bearing USGS geological reference materials including igneous and sedimentary rocks are reported. Calcium isotopic compositions were determined in two laboratories ( GPMR , State Key Laboratory of Geological Processes and Mineral Resources, China University of Geosciences, Wuhan; and CIG , Centre for Isotope Geochemistry, University of California, Berkeley) using the 42 Ca‐ 48 Ca double‐spike technique by thermal ionisation mass spectrometry. As opposed to common cation exchange resin, a micro‐column filled with Ca‐selective resin ( DGA resin) was used in order to achieve high recovery (&gt; 96%) and efficient separation of Ca from the sample matrix. The intermediate measurement precision was evaluated at 0.14‰ (2 s ) for δ 44/40 Ca SRM915a at GPMR , based on replicate measurements of pure Ca reference material NIST SRM 915a, NIST SRM 915b and seawater. Overall, the measurement uncertainties in both laboratories were better than 0.15‰ at the 2 s level. Result validation was carried out for all available data sets. The Ca isotopic compositions of USGS reference materials are not only in agreement between GPMR and CIG , but also in agreement with previously published data within quoted uncertainties. The comprehensive data set reported in this study serves as a reference for both quality assurance and interlaboratory comparison of high precision Ca isotopic study.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Observational · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.392
Threshold uncertainty score0.995

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.001
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0060.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.051
GPT teacher head0.361
Teacher spread0.310 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designObservational
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations80
Published2016
Admission routes1
Has abstractyes

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