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Record W2512760480 · doi:10.15278/isms.2016.tf05

FTIR SYNCHROTRON SPECTROSCOPY OF THE ASYMMETRIC C-H STRETCHING BANDS OF METHYL MERCAPTAN (CH3SH) – A PERPLEXITY OF PERTURBATIONS

2016· article· en· W2512760480 on OpenAlexaffabout
R. M. Lees, Brant Billinghurst, Sylvestre Twagirayezu, David Perry, Mahesh B. Dawadi, Bishnu P. Thapaliya, E.M. Reid, Li‐Hong Xu

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldChemistry
TopicMolecular Spectroscopy and Structure
Canadian institutionsCanadian Light Source (Canada)University of New Brunswick
Fundersnot available
KeywordsPerplexitySynchrotronFourier transform infrared spectroscopySpectroscopyMaterials scienceChemistryPhysicsOpticsComputer scienceAstronomySpeech recognition

Abstract

fetched live from OpenAlex

The infrared Fourier transform spectrum of the asymmetric C-H stretching bands of CH$_{3}$SH has been recorded in the 2950-3100 cm$^{-1}$ region at Doppler limited resolution using synchrotron radiation at the FIR beamline of the Canadian Light Source in Saskatoon. Assignment of numerous torsion-rotation sub-bands for the asymmetric stretches has revealed a surprising pseudo-symmetric behavior, in which each band is seen in only one of the two possible $\\Delta$K selection rules. The upper states of the two asymmetric stretching vibrational bands thus appear to behave more like $\\it{l}$ = $\\pm$ 1 components of a degenerate E state of a symmetric top rather than distinct vibrational states. The two components are separated by about 1.5 cm$^{-1}$ at K = 0, and then diverge linearly at higher K with torsional oscillation amplitude similar to that of the ground state of about 1.3 cm$^{-1}$. The divergence is consistent with an a-type Coriolis splitting picture with an effective Coriolis constant $\\zeta$ $\\approx$ 0.075.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.034
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.236
Teacher spread0.229 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2016
Admission routes2
Has abstractyes

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Same topicMolecular Spectroscopy and StructureFrench-language works237,207