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Record W2517423911 · doi:10.1002/ijch.201600047

Sulfur‐Aromatic Interactions: Modeling Cysteine and Methionine Binding to Tyrosinate and Histidinium Ions to Assess Their Influence on Protein Electron Transfer

2016· article· en· W2517423911 on OpenAlex
Esam A. Orabi

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueIsrael Journal of Chemistry · 2016
Typearticle
Languageen
FieldPhysics and Astronomy
TopicSpectroscopy and Quantum Chemical Studies
Canadian institutionsConcordia UniversityPROTEO
Fundersnot available
KeywordsChemistryElectron transferAromaticityComputational chemistryIonCysteineRedoxHydrogen bondAb initioMethanethiolCrystallographySulfurPhotochemistryInorganic chemistryMoleculeOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Cys and Met interactions with aromatic residues stabilize proteins and also may alter their redox properties. We establish here how ionization of the aromatic groups may influence such interactions. Specifically, ab initio quantum mechanical calculations at the MP2(full)/6‐311++G(d,p) level of theory are performed on the gas‐phase complexes of hydrogen sulfide, methanethiol (MeSH), and dimethyl sulfide (Me 2 S), with the imidazolium and phenolate ions and their 4‐methylated forms. The S‐ligands bind the aromatic ions more tightly than the neutral species, preferentially edge‐on to imidazolium and en‐face to phenolate. Charge transfer occurs within the complexes, which will impact the redox properties of the interacting moieties. The CHARMM36 force field, calibrated using potential energy curves generated at the same level of theory, yields affinities (kcal mol −1 ) in water of −4.3 and −3.1 for MeSH‐ and Me 2 S‐imidazolium, and −2.9 and −2.1 for the phenolate complexes. En‐face binding is preferred in water, with an equilibrium S‐ring‐centroid separation of ∼4 Å, which increases to > 5 Å in Me 2 S‐phenolate. Their high gas‐phase and aqueous stability suggests that S‐aromatic‐ion complexes are an important determinant of protein behavior. Since the uncalibrated CHARMM36 force field predicts very weak S‐aromatic‐ion binding in water (−0.3 to −0.6 kcal mol −1 ) and in the gas phase, the optimized parameters should be used to obtain a reliable description of these interactions in proteins.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.010
Threshold uncertainty score0.441

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.285
Teacher spread0.264 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it