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Record W2555501182 · doi:10.1002/poc.3168

Equilibrium constants for enolization in solution by computation alone

2013· article· en· W2555501182 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueJournal of Physical Organic Chemistry · 2013
Typearticle
Languageen
FieldChemistry
TopicChemical Reaction Mechanisms
Canadian institutionsWestern University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsKeto–enol tautomerismChemistrySolvationEnolAqueous solutionEquilibrium constantThermodynamicsComputational chemistryTautomerPhysical chemistryOrganic chemistryMolecule

Abstract

fetched live from OpenAlex

Equilibrium free energy changes for enolization in aqueous solution can be calculated with useful accuracy (rmse = 1.3 kcal/mol for 37 reactions). These calculations involve gas phase free energy changes calculated using the G3MP2B3 method and solvation energies calculated using the IPCM method corrected by a parameterization scheme which we have reported. For chloroacetones, we find a small preference for enolization to the halogenated side and a preference for forming an enol with Cl Z to the OH. This may be partly due to weak hydrogen bonding but must be partly due to a relief of crowding; 2‐butanone also shows a preference for the Z‐enol. There are serious disagreements between calculated and experimental values for some of the enolization equilibria of 1,3,5‐cyclohexanetrione (phloroglucinol); we argue that the problems are with the experimental values. Reasonable values are obtained for the enolization of Meldrum's acid, diethyl malonate, and 1,3‐cyclohexanedione. Computational equilibrium constants in aqueous solution are now viable as supplements to and checks on experiment. Copyright © 2013 John Wiley & Sons, Ltd.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score0.994

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.243
Teacher spread0.235 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it