MétaCan
Menu
Back to cohort
Record W2558788496 · doi:10.1107/s2053273314083260

Identification of Catalytic Residues in ATP-Citrate Lyase

2014· article· en· W2558788496 on OpenAlexaff
Noreen Singh, Kelsey Holoweckyj, M.E. Fraser

Bibliographic record

VenueActa Crystallographica Section A Foundations and Advances · 2014
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicMetabolism and Genetic Disorders
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsATP citrate lyaseCitrate synthaseBiochemistryLyaseAlanineEnzymeAcetyl-CoACitric acid cycleMalate dehydrogenaseMutantAmino acidBiologyAspartic acidChemistryGene

Abstract

fetched live from OpenAlex

An enzyme in the human body that regulates lipogenesis and cholesterolgenesis is ATP-citrate lyase (ACLY) [1]. ACLY synthesizes acetyl-CoA and oxaloacetate from citrate, CoA and ATP, with citryl-CoA as an intermediate [1]. The product acetyl-CoA is involved in cell growth as well as embryonic and brain development [1]. Studies in mice suggest that ACLY is important during brain development as homozygous Acly knockout mouse embryos died early in development [2]. Knowledge of the reaction mechanism is limited and will be of use in understanding the energy flow in cells. Our current insight into the mechanism by which citryl-CoA is cleaved to form acetyl-CoA and oxaloacetate is based on sequence similarity of ACLY to citrate synthase (CS). Both enzymes have histidine and aspartic acid residues at similar positions in their sequences. We hypothesize that citryl-CoA binds at this site in ACLY and is cleaved into acetyl-CoA and oxaloacetate using these residues. To test this hypothesis, we have mutated these residues to alanine in both human ACLY and ACLY from the bacterium, Chlorobium limicola. Enzymatic activities of the mutant proteins were tested using a coupled-enzyme assay with malate dehydrogenase. The inactive mutants are being used in crystallization trials with substrates, since complexes of the intermediate citryl-CoA can be trapped on the protein. To date, the crystal structure of full-length ACLY has not been published. The structure of only the amino-terminal two-thirds of the human enzyme has been determined [3]; however, the part of the protein that is similar to CS is the carboxy-terminal portion. This work identifies the catalytic residues of ACLY and complements the previous structure determination, increasing our currently limited knowledge about this enzyme.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.950
Threshold uncertainty score0.353

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.248
Teacher spread0.243 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2014
Admission routes1
Has abstractyes

Explore more

Same venueActa Crystallographica Section A Foundations and AdvancesSame topicMetabolism and Genetic DisordersFrench-language works237,207