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Record W2560319282 · doi:10.2451/2016pm655

The crystal structure of mineral fibres: 1. Chrysotile

2016· article· it· W2560319282 on OpenAlexaboutno aff
Simone Pollastri, Natale Perchiazzi, Marco Lezzerini, Jasper R. Plaisier, A. Cavallo, Maria Chiara Dalconi, Nicola Bursi Gandolfi, Alessandro F. Gualtieri

Bibliographic record

VenueCINECA IRIS Institutial research information system (University of Pisa) · 2016
Typearticle
Languageit
FieldMaterials Science
TopicGraphite, nuclear technology, radiation studies
Canadian institutionsnot available
FundersUniversità di PisaUniversità degli Studi di Trento
KeywordsChrysotileEMPAOctahedronPowder diffractionCrystal structureMaterials scienceCrystallographyMineralX-ray crystallographyMineralogyElectron microprobeChemistryDiffractionMetallurgyOpticsPhysics

Abstract

fetched live from OpenAlex

This work reports the results of the structural study of three representative chrysotile samples of different provenance (Canadian UICC, and Italian Balangero and Valmalenco). Chemical composition was determined using EMPA and TG data. An innovative wet cryo-milling procedure was used to powder the flexible and durable chrysotile fibres. X-ray powder diffraction patterns were collected using both conventional and nonconventional sources. Collected data were used for Rietveld structural refinements and results were compared with available literature data. The three samples display similar structure models, although small differences were detected in the position of the oxygen atoms. Both the structural refinements and spectroscopic investigations confirms that Fe2+ and Fe3+ atoms in chrysotile are located in the octahedral cavities only, substituting for Mg2+. Regarding the atom coordinates, UICC chrysotile is the closest to the model reported by Falini et al. (2004). About the lattice parameters, the Valmalenco chrysotile is the closest, if compared with the Balangero and UICC, to both the model proposed by Whittaker (1956a,b) and Falini et al. (2004). This work is intended as a basis for subsequent studies aimed at understanding the toxicity of these mineral fibres.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.066
Threshold uncertainty score0.130

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0010.000
Scholarly communication0.0010.000
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.032
GPT teacher head0.266
Teacher spread0.234 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designNot applicable
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations23
Published2016
Admission routes1
Has abstractyes

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