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Record W2576251728 · doi:10.1002/cjce.22786

Optimization of supercritical fluid extraction of isoflavone from soybean meal

2017· article· en· W2576251728 on OpenAlexaffvenue
Kanjana Lummaetee, Hong‐Ming Ku, Wongphaka Wongrat, Ali Elkamel

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2017
Typearticle
Languageen
FieldEngineering
TopicPhase Equilibria and Thermodynamics
Canadian institutionsUniversity of Waterloo
Fundersnot available
KeywordsSupercritical carbon dioxideSupercritical fluid extractionSupercritical fluidExtraction (chemistry)Mass transferChromatographyMass transfer coefficientSolubilityMethanolCarbon dioxideChemistryThermal diffusivityMaterials scienceThermodynamicsOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract This study aims at developing a mathematical model to predict the yield of isoflavone from soybean meal in a supercritical extraction process using carbon dioxide and aqueous methanol as a co‐solvent and to optimize the process using a genetic algorithm. In the model, a partial differential equation based conservation of mass was solved to predict the yield of isoflavone extraction. The model parameters such as densities of carbon dioxide and co‐solvent methanol, the mixture viscosity, the binary diffusion coefficient of isoflavone in the supercritical solvents, the film mass transfer coefficient, effective diffusivity, and axial dispersion coefficient were estimated using available correlations, and the solubility was estimated using the Mohsen‐Nia‐Moddaress‐Mansoori equation of state. The model was successfully validated with experimental data. In the optimization, the operating conditions of the isoflavone extraction process were identified as decision variables and a profit function was maximized. The optimum was found under the condition in which the carbon dioxide flow rate was 5.88 kg/h and the particle diameter was 0.68 mm, when the temperature was 323.15 K, the pressure was 59.45 MPa, and the extraction time was 283 min. The maximum profit found under these optimum conditions was 46.18 $ per batch.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.330
Threshold uncertainty score0.345

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.205
Teacher spread0.196 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations14
Published2017
Admission routes2
Has abstractyes

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