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Record W2576955998

Design of Functionalized Cellulose Nanocrystals for Personal Care Applications

2017· dissertation· en· W2576955998 on OpenAlexaboutno aff
Fatima Awan

Bibliographic record

VenueUWSpace (University of Waterloo) · 2017
Typedissertation
Languageen
FieldMaterials Science
TopicAdvanced Cellulose Research Studies
Canadian institutionsnot available
Fundersnot available
KeywordsCelluloseNanocrystalNanotechnologyMaterials scienceEngineeringChemical engineering
DOInot available

Abstract

fetched live from OpenAlex

Derived from the depths of rich, green Canadian forests; the discovery of cellulose nanocrystals (CNCs) has pushed the research and industrial community to find strategic alternatives to replace existing non-renewable building blocks. With the commissioning of world’s largest CNC demonstration plant in Quebec, Canada, the utilization of cellulose nanocrystals is feasible, and has opened a myriad of applications in recent years, such as energy, sensors, water treatment, biometrics, photonics etc. \nThis dissertation describes the modification of fundamentally inactive CNCs, and converting them into colloidally-active cosmetic systems. In the first approach, the high surface area, and equatorial -OH groups of CNCs were utilized for the nucleation of polyhydroxylated C60 fullerene, as a new antioxidant. The reaction kinetics were quantified and fitted to a pseudo first-order model, and a 2–stage biomolecular reaction mechanism was proposed. This work directly addresses the issue of insolubility that has previously hindered the biological application of the carbon nanocage (C60/C70), and has direct implications for understanding the underlying mechanism of the reaction-kinetics. \nAt the nanoscale, the surface properties become more dominant than in the bulk-phase due to the relatively higher proportion of atoms at the particle surface. Here, in the second approach a nitrogen-rich porous CNC template enabled the confined growth of semiconductor ZnO, providing a proportionally higher curvature to enhance the active catalytic sites on the metal oxide. The hybrid system was evaluated for in-vitro sun protection factor (SPF) and photocatalytic activity under UV and solar stimulation, and interpreted through the solid-band theory. The reaction kinetics were fit to the Langmuir-Hinshelwood model displaying a 4-fold increase in the photocatalytic activity of the hybrid nanostructure, compared to pure ZnO. Our work suggests that an increase in photocatalysis can be engineered without the introduction of structural defects or tailoring the band gap of ZnO. \nTo the best of our knowledge, this thesis represents one of the first pioneering studies that reports on the development of optimized personal care systems derived from fCNCs. Our studies showed that the translation of this renewable nanomaterial into scalable cosmetic systems is suggestively viable.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.027
GPT teacher head0.265
Teacher spread0.239 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2017
Admission routes1
Has abstractyes

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