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Record W2793164271 · doi:10.1002/cjce.23192

Photo‐catalytic degradation of formaldehyde using nitrogen‐doped TiO<sub>2</sub> nano‐photocatalyst: Statistical design with response surface methodology (RSM)

2018· article· en· W2793164271 on OpenAlexvenueno aff
Maryam Mirzaei, Samad Sabbaghi, M. M. Zerafat

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2018
Typearticle
Languageen
FieldEnvironmental Science
TopicWater Quality Monitoring and Analysis
Canadian institutionsnot available
Fundersnot available
KeywordsFormaldehydePhotocatalysisResponse surface methodologyCatalysisMaterials scienceCentral composite designFourier transform infrared spectroscopyDegradation (telecommunications)Nuclear chemistryNano-NitrogenNanoparticleChemical engineeringSpectrophotometryDopingChemistryNanotechnologyComposite materialChromatographyOrganic chemistryOptoelectronics

Abstract

fetched live from OpenAlex

Abstract Formaldehyde is considered as a common pollutant in industrial wastewaters requiring removal techniques designed to reduce its harmful effects due to distribution in the environment. In this study, TiO2 nanoparticles are modified through nitrogen doping by sol‐gel technique and their photo‐catalytic performance for formaldehyde degradation is studied under UV and solar irradiation. Various characterization techniques such as: PSA, FTIR, XRD, and SEM are performed on the synthesized nano‐photocatalyst with a ∼20 nm average size. The significance of parameters such as initial formaldehyde concentration, catalyst molar ratio N/Ti, pH, and removal time under UV and solar radiation are assessed using response surface methodology based on central composite design. Formaldehyde removal was measured as a function of irradiation time using UV‐Visible spectrophotometry. The results show that the maximum formaldehyde removal at optimal conditions (pH = 5 for 400 ppm initial formaldehyde concentration) by nitrogen‐doped TiO2 is 64.02 % under solar and 60.15 % under UV radiation suggesting it as an effective photo‐catalyst for formaldehyde removal.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.003
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.016

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0030.003
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.045
GPT teacher head0.250
Teacher spread0.205 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations28
Published2018
Admission routes1
Has abstractyes

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