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Record W2795797350 · doi:10.1149/2.0951805jes

Synthesis of Single Crystal LiNi<sub>0.6</sub>Mn<sub>0.2</sub>Co<sub>0.2</sub>O<sub>2</sub>with Enhanced Electrochemical Performance for Lithium Ion Batteries

2018· article· en· W2795797350 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueJournal of The Electrochemical Society · 2018
Typearticle
Languageen
FieldEngineering
TopicAdvancements in Battery Materials
Canadian institutionsDalhousie University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsCrystalliteElectrolyteLithium (medication)Materials scienceSingle crystalElectrochemistrySinteringCrystal (programming language)IonLithium carbonateBattery (electricity)Chemical engineeringAnalytical Chemistry (journal)Inorganic chemistryElectrodeChemistryCrystallographyMetallurgyPhysical chemistryIonic bonding

Abstract

fetched live from OpenAlex

Single crystal LiNi0.5Mn0.3Co0.2O2 (NMC532) was shown to have superior stability at high voltages and elevated temperatures compared to conventional polycrystalline NMC532 by the authors. Conventional LiNi0.6Mn0.2Co0.2O2 (NMC622) usually offers more capacity than NMC532 when charged to the same upper cutoff voltage so NMC622 is attractive. It is expected that single crystal NMC622 could also provide better performance than typical polycrystalline NMC622 materials. This work explores the synthesis of single crystal LiNi0.6Mn0.2Co0.2O2 and preferred synthesis conditions were found. A washing and reheating method was used to remove residual lithium carbonate after sintering. The synthesized single crystal NMC622 material worked poorly after the washing-heating treatment without the use of electrolyte additives in the electrolyte. However, with selected additives, single crystal cells outperformed the polycrystalline reference cells in cycling tests. It is our opinion that single crystal NMC622 has a bright future in the Li-ion battery field.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.032
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.214
Teacher spread0.207 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it