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Record W2808368318

Electrochemical study and corrosion modeling of chromium alloy steels exposed to sulfide containing environment

2018· dissertation· en· W2808368318 on OpenAlexfundno aff
Ladan Khaksar

Bibliographic record

VenueMemorial University Research Repository (Memorial University) · 2018
Typedissertation
Languageen
FieldMaterials Science
TopicCorrosion Behavior and Inhibition
Canadian institutionsnot available
FundersMemorial University of NewfoundlandSuncor Energy Incorporated
KeywordsCorrosionAlloyMaterials scienceMetallurgySulfideSour gasSulfurChromiumElectrochemistryScanning electron microscopeIron sulfideMetalAlloy steelComposite materialChemistryElectrode
DOInot available

Abstract

fetched live from OpenAlex

Corrosion, the destructive result of a chemical reaction between a metal or metal alloy and its environment in sour systems (H₂S dominant) has progressively become a greater concern to the oil and gas industry as a result of production from increasingly sour environments. In this study, the effects of the principal H₂S corrosion product, iron sulfide, on the corrosion resistance of alloy steel were initially investigated, followed by the study of the corrosion behavior of alloy steels in the presence of elemental sulfur, which is often present in sour systems. A new experimental method was applied to synthesize the iron sulfide layer on the steel surface with no H₂S in the environment. Attempts were also made to develop an accurate computational model to predict the corrosion rate of alloy steel in various environmental conditions. A series of experiments was performed to study chloride concentration, temperature, immersion time and pH effects on the corrosion behavior of alloy steel in the simulated sour environment. Various analyzing methods, such as scanning electron microscopy and X-ray diffraction, were applied to investigate the results which suggest that each factor can significantly affect the electrochemical behavior of alloy steel, especially in the presence of H₂S corrosion products. The corrosion of alloy steel in the presence of elemental sulfur was also studied using the cyclic polarization technique. In general, it was shown that the presence of deposited layers of elemental sulfur on the surface of 13% Cr steel will increase the corrosion rate by decreasing the scaling tendency of corrosion products on the surface, especially at higher temperature. The experimental data were analyzed and used to develop an analytical model to show the effects of corrosion products, chloride concentration, pH and temperature on the likelihood of corrosion of 13% chromium steel.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score0.016

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.032
GPT teacher head0.270
Teacher spread0.238 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2018
Admission routes1
Has abstractyes

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