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Record W2823631200 · doi:10.1021/acs.inorgchem.8b01208

H<sub>2</sub>hox: Dual-Channel Oxine-Derived Acyclic Chelating Ligand for <sup>68</sup>Ga Radiopharmaceuticals

2018· article· en· W2823631200 on OpenAlexafffund
Xiaozhu Wang, Marı́a de Guadalupe Jaraquemada-Peláez, Yang Cao, Jinhe Pan, Kuo‐Shyan Lin, Brian O. Patrick, Chris Orvig

Bibliographic record

VenueInorganic Chemistry · 2018
Typearticle
Languageen
FieldMedicine
TopicRadiopharmaceutical Chemistry and Applications
Canadian institutionsBC Cancer AgencyUniversity of British Columbia
FundersNatural Sciences and Engineering Research Council of CanadaCanadian Institutes of Health Research
KeywordsChemistryLigand (biochemistry)ChelationGalliumFluorescenceHox geneIn vivoPositron emission tomographyRadiochemistryAnalytical Chemistry (journal)ChromatographyInorganic chemistryReceptorNuclear medicineOrganic chemistryBiochemistry

Abstract

fetched live from OpenAlex

An acyclic hexadentate oxine-derived chelating ligand, H 2 hox, was investigated as an alternative to current chelators for 68 Ga. The straightforward preparation of H 2 hox, involving only one or two steps, obviates the synthetic challenges associated with many reported 68 Ga chelators; it forms a Ga 3+ complex of great stability (log K = 34.4) with a remarkably high gallium scavenging ability (pGa 3+ = −log[Ga 3+ free ] = 28.3, ([Ga 3+ ] = 1 μM; [L x – ] = 10 μM; pH 7.4, and 25 °C)). Moreover, H 2 hox coordinates 68 Ga quantitatively in 5 min at room temperature in ligand concentrations as low as 1 × 10 –7 M, achieving an unprecedented high molar activity of 11 ± 1 mCi/nmol (407 ± 3.7 MBq/nmol) without purification, suggesting prospective kit-based convenience. [ 68 Ga(hox)] + showed no decomposition in a plasma challenge. Good in vivo stability and fast renal and hepatic clearance of the [ 68 Ga(hox)] + complex were demonstrated using dynamic positron emission tomography/computed tomography imaging. The intrinsic fluorescence of [Ga(hox)] + allowed for direct fluorescence imaging of cellular uptake and distribution, demonstrating the dual-channel detectability and intracellular stability of the metal complex.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.005

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.029
GPT teacher head0.314
Teacher spread0.285 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations30
Published2018
Admission routes2
Has abstractyes

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