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Record W2883314322 · doi:10.1107/s1600576718008737

Determination of temperature-dependent crystallographic parameters of Al–Si alloys using <i>in situ</i> neutron diffraction

2018· article· en· W2883314322 on OpenAlexafffund
Eli Vandersluis, D. Sediako, Payam Emadi, C. Ravindran, Abdallah Elsayed, Glenn Byczynski

Bibliographic record

VenueJournal of Applied Crystallography · 2018
Typearticle
Languageen
FieldEngineering
TopicAluminum Alloy Microstructure Properties
Canadian institutionsMagna International (Canada)Canadian Nuclear LaboratoriesUniversity of British Columbia, Okanagan CampusUniversity of GuelphUniversity of British ColumbiaToronto Metropolitan University
FundersNatural Sciences and Engineering Research Council of CanadaCanadian Nuclear LaboratoriesUniversity of Toronto
KeywordsEutectic systemThermal expansionNeutron diffractionMaterials scienceAlloyLattice constantDiffractionLattice (music)Atmospheric temperature rangeIn situSolid solutionCrystallographyX-ray crystallographyAnalytical Chemistry (journal)Crystal structureThermodynamicsMetallurgyChemistry

Abstract

fetched live from OpenAlex

Accurate evaluation of temperature-dependent lattice spacings of individual phases in complex engineering alloys enables analysis and design of enhanced components for high-temperature applications. However, typical characterization techniques are limited to measurements at temperatures at which the alloy is completely solid state. In this study, in situ neutron diffraction was performed to determine the crystallographic parameters of several phases in unmodified and Sr-modified Al–6 wt% Si and A319 alloys from the start of solidification to 423 K. Approximately linear correlations were found for the interplanar spacings and lattice parameters of Al, Si, Al 5 Mg 8 Cu 2 Si 6 and Al 15 (Fe,Mn) 3 Si 2 phases with temperature for the entire measured range. The greater concentration of lattice-contracting elements dissolved in the A319 solid solutions resulted in smaller lattice spacings and larger coefficients of thermal expansion than the same phases in Al–6 wt% Si, yet eutectic modification with Sr did not produce noticeable changes in the crystallographic parameters. The Si phase was found to have the largest thermal expansion coefficient misfit with the Al matrix. These findings offer significant insight into the development and mitigation of thermal stresses in the processing and operation of engineering components.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.028
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.212
Teacher spread0.204 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations6
Published2018
Admission routes2
Has abstractyes

Explore more

Same venueJournal of Applied CrystallographySame topicAluminum Alloy Microstructure PropertiesFrench-language works237,207