Direct observation of dislocation nucleation in pyrite using combined electron channelling contrast imaging and electron backscatter diffraction
Bibliographic record
Abstract
Abstract Crystal‐plastic deformation is one of the main mechanisms that can accommodate large amounts of strain within the lithosphere. Despite the requirement of understanding dislocation nucleation and arrangement, the only accepted method for direct observation of dislocations in geological materials so far is transmission electron microscopy. Herein, we present a study using a combination of electron channelling contrast imaging (ECCI) and electron backscatter diffraction (EBSD) to visualize and analyse crystal defects in pyrite deforming close to the crystal plastic to brittle transition zone. Structures in focus include (a) dislocation nucleation at crack‐tips and (b) the reactivation of mode I cracks accompanied by the nucleation of dislocations and crystal‐plastic behaviour resulting in the development of complex dislocation structures and low‐angle grain boundaries. EBSD maps reveal an increase in misorientation towards micro‐cracks, consistent with a greater dislocation density along cracks observed by ECCI.
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How this classification was reachedexpand
Full frame machine prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.
Distilled classifier scores by category (both heads)
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.001 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.001 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".