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Record W2911218807 · doi:10.1002/cjce.23445

Production of isophthalic acid from M‐Xylene catalyzed by Co(II) and HPW@C modified with ZnCl<sub>2</sub> solution

2019· article· en· W2911218807 on OpenAlexvenueno aff
Zhihao Wang, Hua‐jie Liu, Zhou‐wen Fang, Xin‐zhi Zhou, Xiang‐li Long

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2019
Typearticle
Languageen
FieldChemistry
TopicNanomaterials for catalytic reactions
Canadian institutionsnot available
FundersNational Natural Science Foundation of China
KeywordsPhosphotungstic acidIsophthalic acidCatalysisCarbonizationCarbon fibersChemistryActivated carbonXyleneNuclear chemistryInorganic chemistryOrganic chemistryMaterials scienceTerephthalic acidAdsorptionBenzene

Abstract

fetched live from OpenAlex

Abstract The production of isophthalic acid (IPA) from the oxidation of m‐xylene (MX) with air can be sped up by Co(II) and phosphotungstic acid (HPW) loaded on activated carbon. In this paper, activated carbon is modified with a ZnCl 2 solution to improve the catalytic performance of the HPW@C catalyst. The experiments indicate that the optimum modification condition is the carbon immersed in a 0.10 mol L −1 ZnCl 2 solution for 6 h at the temperature of 40 °C followed by being carbonized at 600 °C for 4 h. The characterization proves that the ZnCl 2 modification leads to the increase of surface area and acidic groups on the activated carbon. The MX conversion catalyzed by the HPW@C prepared from the carbon modified is 7.0 % over that by the HPW@C from the original carbon and the IPA produced by the modified sample is 78.9 % over that produced by the original one.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.465

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.172
Teacher spread0.167 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2019
Admission routes1
Has abstractyes

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