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Record W2913916728 · doi:10.1111/febs.14784

Crystal structures of human 17β‐hydroxysteroid dehydrogenase type 1 complexed with estrone and <scp>NADP</scp><sup>+</sup> reveal the mechanism of substrate inhibition

2019· article· en· W2913916728 on OpenAlexafffund
Tang Li, Preyesh Stephen, Dao‐Wei Zhu, Rong Shi, Sheng‐Xiang Lin

Bibliographic record

VenueFEBS Journal · 2019
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicEstrogen and related hormone effects
Canadian institutionsUniversité Laval
FundersCanadian Institutes of Health Research
KeywordsDehydrogenaseCofactorEnzymeEstroneChemistry11β-hydroxysteroid dehydrogenase type 1Ternary complexStereochemistrySubstrate (aquarium)Hydroxysteroid dehydrogenaseBiochemistryBiology

Abstract

fetched live from OpenAlex

Human 17β‐hydroxysteroid dehydrogenase type 1 (17β‐ HSD 1) catalyses the last step in estrogen activation and is thus involved in estrogen‐dependent diseases ( EDD s). Unlike other 17β‐ HSD members, 17β‐ HSD 1 undergoes a significant substrate‐induced inhibition that we have previously reported. Here we solved the binary and ternary crystal structures of 17β‐ HSD 1 in complex with estrone (E1) and cofactor analog NADP + , demonstrating critical enzyme‐substrate‐cofactor interactions. These complexes revealed a reversely bound E1 in 17β‐ HSD 1 that provides the basis of the substrate inhibition, never demonstrated in estradiol complexes. Structural analysis showed that His 221 is the key residue responsible for the reorganization and stabilization of the reversely bound E1, leading to the formation of a dead‐end complex, which exists widely in NADP (H)‐preferred enzymes for the regulation of their enzymatic activity. Further, a new inhibitor is proposed that may inhibit 17β‐ HSD 1 through the formation of a dead‐end complex. This finding indicates a simple mechanism of enzyme regulation in the physiological background and introduces a pioneer inhibitor of 17β‐ HSD 1 based on the dead‐end inhibition model for efficiently targeting EDD s. Databases Coordinates and structure factors of 17β‐ HSD 1‐E1 and 17β‐ HSD 1‐E1‐ NADP + have been deposited in the Protein Data Bank with accession code 6MNC and 6MNE respectively. Enzymes 17β‐hydroxysteroid dehydrogenase type 1 (17β‐ HSD 1) EC 1.1.1.62 .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.460

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.216
Teacher spread0.209 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations29
Published2019
Admission routes2
Has abstractyes

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