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Hydrotreatment of Olefins in Thermally Processed Bitumen under Mild Conditions

2019· article· en· W2923219332 on OpenAlexafffund
Qin Xin, Anton Alvarez‐Majmutov, Rafał Gieleciak, Jinwen Chen, Heather D. Dettman

Bibliographic record

VenueEnergy & Fuels · 2019
Typearticle
Languageen
FieldChemistry
TopicPetroleum Processing and Analysis
Canadian institutionsNatural Resources Canada
FundersNatural Resources Canada
KeywordsHydrodesulfurizationNaphthaOlefin fiberAsphaltFraction (chemistry)ChemistryOrganic chemistryOil sandsRaw materialCatalysisChemical engineeringMaterials scienceComposite material

Abstract

fetched live from OpenAlex

The stabilization of olefins in a thermally processed bitumen is a focal area for the development of bitumen partial upgrading technologies. Although a number of approaches have been proposed, including alkylation, oligomerization, and adsorption, hydrotreatment is still the most effective strategy for treating olefins in thermally cracked products such as coker naphtha. In our previous work, we studied the hydrogenation of model olefin compounds to understand their reactivity under mild conditions. This paper is a follow-up study focusing on the hydrotreatment of olefins in a thermally processed bitumen using a bench-scale continuous hydroprocessing unit. Two different scenarios were investigated: (1) hydrotreating the olefin-rich light fraction (IBP-280 °C) of the thermally processed bitumen product and (2) hydrotreating the whole product. The cracked feedstock was prepared by processing oil sand bitumen under visbreaking conditions. It was found that on-specification product for olefin content (<1.0 wt % 1-decene equivalent) could be obtained by hydrotreating the light fraction at lower temperatures (∼275–300 °C) and with less hydrogen as compared to hydrotreating the whole bitumen product, for which temperatures close to 325 °C are required in addition to about double the hydrogen input. Hydrotreating the whole product, however, brings the benefit of markedly reducing the total acid number and increasing the American Petroleum Institute gravity, which can be helpful to achieve the product quality goals of partial upgrading. Product characterization by advanced techniques such as 1H NMR and two-dimensional gas chromatography has revealed interesting reactivity patterns of olefins, sulfur compounds, and aromatics during mild hydrotreatment.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.061
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.234
Teacher spread0.225 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations19
Published2019
Admission routes2
Has abstractyes

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