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Record W2951260887 · doi:10.1021/ic040034y

Zr<sub>7</sub>Sb<sub>4</sub>:  A New Binary Zirconium-Rich Antimonide

2004· article· en· W2951260887 on OpenAlexaff
Andriy V. Tkachuk, Arthur Mar

Bibliographic record

VenueInorganic Chemistry · 2004
Typearticle
Languageen
FieldChemistry
TopicInorganic Chemistry and Materials
Canadian institutionsUniversity of Alberta
Fundersnot available
KeywordsAntimonideChemistryAntimonyCrystallographyZirconiumMonoclinic crystal systemTetragonal crystal systemCrystal structureGroup (periodic table)Annealing (glass)X-ray crystallographyFormula unitDiffractionInorganic chemistryMetallurgyMaterials science

Abstract

fetched live from OpenAlex

Zr(7)Sb(4) has been prepared by arc-melting of the elemental components and annealing at 1000-1150 degrees C. Its crystal structure was determined by X-ray diffraction (Pearson symbol mP44, monoclinic, space group P2(1)/c, Z = 4, a = 8.4905(6) A, b = 11.1557(8) A, c = 11.1217(8) A, beta = 111.443(2) degrees at 295 K). Zr(7)Sb(4) is isotypic to Hf(6)TiSb(4), a compound stabilized by differential fractional site occupancy. It is the first binary group-4 antimonide with this metal-to-antimony ratio, but it differs from the corresponding phosphides and arsenides M(7)Pn(4) (M = Ti, Zr, Hf; Pn = P, As), which adopt the Nb(7)P(4)-type structure. Zr(7)Sb(4) is built up from layers excised from the tetragonal W(5)Si(3)-type structure; these layers are displaced relative to each other to maximize interlayer Zr-Zr and Zr-Sb bonding, as confirmed by band structure calculations.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Research integrity, Insufficient payload (model declined to judge)
Consensus categoriesInsufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.010
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0030.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.205
Teacher spread0.197 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; both teacher heads agree on what is shown here.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2004
Admission routes1
Has abstractyes

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