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Record W2951719842 · doi:10.1021/ic062277r

Ternary Zirconium Tin Antimonide ZrSn<sub>2</sub><sub>-</sub><i><sub>x</sub></i>Sb<i><sub>x</sub></i> (0.2 &lt; <i>x</i> &lt; 0.8), Different from the Parent Binaries ZrSn<sub>2</sub> and ZrSb<sub>2</sub>

2007· article· en· W2951719842 on OpenAlexaff
Andriy V. Tkachuk, Davin G. Piercey, Arthur Mar

Bibliographic record

VenueInorganic Chemistry · 2007
Typearticle
Languageen
FieldChemistry
TopicInorganic Chemistry and Materials
Canadian institutionsUniversity of Alberta
Fundersnot available
KeywordsAntimonideChemistryTinZirconiumTernary operationAntimonyCrystallographyX-ray crystallographyInorganic chemistryPhysicsDiffractionOptics

Abstract

fetched live from OpenAlex

The new intermetallic phase ZrSn2-xSbx was prepared by arc-melting and annealing at 800 degrees C. It adopts the hexagonal CrSi2-type structure (Pearson symbol hP9, space group P6222 (or P6422), Z = 3, a = 5.51-5.53 A, c = 7.65-7.63 A) and exhibits a significant phase width (0.2 < x < 0.8). In contrast, the parent binary phases adopt different structures: ZrSn2 has the orthorhombic TiSi2-type structure, and ZrSb2 exists as two orthorhombic forms (alpha-ZrSb2, own type; "beta-ZrSb2", PbCl2-type). The structures of ZrSn2, ZrSn2-xSbx, and beta-ZrSb2 are distinguished by the stacking and distortion of nets with composition "ZrQ2" (Q = Sn, Sb). The CrSi2-type and TiSi2-type structures differ only minimally in energy, but interlayer Sb-Sb bonding is important in stabilizing the structure of beta-ZrSb2.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.002
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies, Scholarly communication, Open science, Research integrity, Insufficient payload (model declined to judge)
Consensus categoriesMeta-epidemiology (narrow), Science and technology studies, Research integrity
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.019
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0030.002
Meta-epidemiology (narrow)0.0070.007
Meta-epidemiology (broad)0.0060.002
Bibliometrics0.0000.002
Science and technology studies0.0030.003
Scholarly communication0.0020.002
Open science0.0060.005
Research integrity0.0050.006
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.201
Teacher spread0.193 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; both teacher heads agree on what is shown here.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2007
Admission routes1
Has abstractyes

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