Synthesis and Crystal Structure of Pd<sub>5</sub>InSe
Bibliographic record
Abstract
Pd 5 InSe has been prepared from the elements. The use of iodine as a mineralizing agent enables the synthesis of single-phase powder samples as well as of single crystals. Pd 5 InSe is stable in cold air, but reacts to give Pd, In 2 O 3 and Pd 4 Se at 400 °C. The crystal structure of Pd 5 InSe was determined from single-crystal X-ray diffraction data (space group P4=mmm, a = 4.0255(7), c = 6.972(1) Å, z(Pd2) = 0.28111(8)) and belongs to the Pd 5 TlAs-type structure with full occupation of all atomic sites. EDX analysis on the single crystal (Pd 5.0 (1)In 0.99 (3)Se 1.0 (1)) confirms the stoichiometric composition. The relationship to the cubic close packing (Cu-type structure), which may be visualized by the crystal chemical formula Pd 4 PdTlAs⃞, is proven by a Bärnighausen symmetry tree.
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How this classification was reachedexpand
Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.001 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.001 | 0.000 |
| Insufficient payload (model declined to judge) | 0.001 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one teacher head, not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".