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Record W2955551274 · doi:10.1021/acs.macromol.9b00910

Highly Ordered Sub-10 nm Patterns Based on Multichain Columns of Side-Chain Liquid Crystalline Polymers

2019· article· en· W2955551274 on OpenAlex
Xu‐Qiang Jiang, Ruiying Zhao, Wen-Ying Chang, Dongxiao Yin, Yechang Guo, Wei Wang, Dehai Liang, Shuang Yang, An‐Chang Shi, Er‐Qiang Chen

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueMacromolecules · 2019
Typearticle
Languageen
FieldMaterials Science
TopicBlock Copolymer Self-Assembly
Canadian institutionsMcMaster University
FundersMinistry of Science and Technology of the People's Republic of ChinaFudan UniversityNational Natural Science Foundation of China
KeywordsSide chainPolymerMaterials scienceShearing (physics)NanotechnologyPhase (matter)Liquid crystallineNanostructureSelf-assemblyMesogenCrystallographyComposite materialChemistryOrganic chemistry

Abstract

fetched live from OpenAlex

The development of nanotechnology relies crucially on the ability to fabricate materials with desired nanostructures. Because of their precise side-chain structure and versatile ordered morphologies, side-chain liquid crystalline polymers can provide a novel material platform to obtain sub-10 nm structures via their self-assembly. Here we show that for a newly designed side-chain liquid crystalline (LC) polynorbornene (P1) with a slim hemiphasmid mesogen microphase separation between the main and side chains drives the spontaneous formation of hexagonal columnar phase (Φh) composed of cylinders with a uniform diameter of 8.3 nm. At every cross section of the cylinder there are more than a dozen P1 chains laterally bundled together. The cylinders can grow axially when more chains join in becoming extraordinarily long to over several micrometers. Simple shearing can produce P1 thin films with very good orientation of the Φh phase at the macroscopic scale. More interestingly, we show that directed self-assembly of graphoepitaxy of P1 also provides an efficient route to obtain the patterned cylinders, making its applications in nanotechnology highly possible.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.218
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it