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Record W3012563719 · doi:10.1139/cjc-2019-0464

A quantum chemical study of encapsulation and stabilization of gallic acid in <i>β</i>-cyclodextrin as a drug delivery system

2020· article· en· W3012563719 on OpenAlexvenueno aff
Oukacha Guendouzi, Abdelkrim Guendouzi, H. B. Ouici, Houari Brahim, Mostefa Boumediene, Mohammed Elkeurti

Bibliographic record

VenueCanadian Journal of Chemistry · 2020
Typearticle
Languageen
FieldChemistry
TopicCrystallography and molecular interactions
Canadian institutionsnot available
Fundersnot available
KeywordsChemistryNatural bond orbitalSupermoleculeDensity functional theoryComputational chemistryCyclodextrinHydrogen bondGallic acidAqueous solutionMolecular dynamicsSolubilityHydrophobic effectCombinatorial chemistryOrganic chemistryMolecule

Abstract

fetched live from OpenAlex

This research paper describes the study of the inclusion complex formation of a 1:1 stoichiometry ratio of host–guest inclusion complex (X-β-CD) between gallic acid (GA), which is reported to have anti-cancer effects, and β-cyclodextrin (β-CD). The use of β-CD for the encapsulation of bioactive compounds can protect the drugs against conjugation and metabolic inactivation and improve the aqueous solubility for increasing their capacity to functionalize the products. The objective of this study is to give insight on the mechanism of complexation and the capability of β-CD to encapsulate GA compound (X) in gas and solution phases. We examine and compare the performances of different quantum mechanical methods, namely HF/6-31G* and density functional theory (DFT; B97D3/6-31G* functional including dispersion correction), to study the importance of the contribution of the dispersion forces and the hydrogen bonding in the mechanism of interaction. The stability of the optimized geometries of the complex was evaluated with the supermolecule method. Two modes of complexation are taken into consideration. Moreover, the inclusion complex can be confirmed using the frontier molecular orbital (FMO) theory, the global indices of reactivity, the electronic populations condensed natural bond orbital (NBO) analysis, and the molecular docking, which examine the quality and the nature of the hydrophobic interactions during the complexation process.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.017
Threshold uncertainty score0.479

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.205
Teacher spread0.197 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations16
Published2020
Admission routes1
Has abstractyes

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