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Record W3034221017 · doi:10.1039/d0nr01653e

Highly selective and sensitive fluorescent zeolitic imidazole frameworks sensor for nitroaromatic explosive detection

2020· article· en· W3034221017 on OpenAlexafffund
Osama Abuzalat, Danny Wong, Simon S. Park, Seonghwan Kim

Bibliographic record

VenueNanoscale · 2020
Typearticle
Languageen
FieldChemistry
TopicMetal-Organic Frameworks: Synthesis and Applications
Canadian institutionsCalgary Laboratory ServicesUniversity of Calgary
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsExplosive materialImidazoleFluorescenceExplosive detectionMaterials scienceNanotechnologyCombinatorial chemistryChemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Nitroaromatic explosives, such as 2-4-6 trinitrotoluene (TNT) are dangerous materials that pose safety and environmental risks. Even though many sensors have been reported for the detection of nitroaromatic explosives, a facile, rapid, cost-effective sensor is still sought-after in the field. Here we demonstrate a facile and rapid method to synthesize a fluorescent metal-organic framework for the highly selective and sensitive detection of nitroaromatic explosives. Zeolitic imidazole framework-8 (ZIF-8) is synthesized and enhanced with fluorescent 8-hydroxyquinoline zinc (ZnQ). The synthesized material shows visible colour changes upon exposure to TNT from ivory to light red. In addition, fluorescence quenching is noted under UV illumination when the ZnQ@ZIF-8 is exposed to TNT. The ZnQ@ZIF-8-coated paper sensors show the highest fluorescence quenching at an emission wavelength of 455 nm with TNT concentration as low as 1 ppm. Therefore, the proposed strategy not only offers a fast and convenient protocol for selective detection of TNT but also offers great potential in practical applications, especially for airport/railway security inspection and prevention of terrorist attacks.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.046
Threshold uncertainty score0.954

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.227
Teacher spread0.214 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations77
Published2020
Admission routes2
Has abstractyes

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