Sol-gel synthesis and characterization of MgSO4:Mg(NO3)2 – Al2O3 composite solid elec-trolytes
Bibliographic record
Abstract
Composite solid electrolytes in the system (1-x)MgSO 4 :Mg(NO 3 ) 2 -xAl 2 O 3 with x = 0.1-0.6 were synthesized by sol-gel method and analysed by X-ray diffraction, differential scanning calorimetry, scanning electron microscopy, energy dispersive X-ray, Fourier transform infrared spectroscopy and alternating current impedance spectroscopy. Structural analysis revealed solid-solid phase transformation of anhydrous MgSO 4 to -MgSO 4 after sintering at 900 C for 2 hours. Recrystallization of crystalline -MgSO 4 phase was observed for composite samples with x = 0.1 -0.3. Addition of anhydrous MgSO 4 and Mg(NO 3 ) 2 as a co-host, resulted in the formation of MgO phase after heat treatment. The conductivities of the composites were in the order of 10-7 S cm -1 at room temperature on account from the formation of a new region of Mg 2 +|MgO.
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How this classification was reachedexpand
Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.001 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.001 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.000 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one teacher head, not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".