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Record W3098977393 · doi:10.1180/mgm.2020.88

Manganoarrojadite-(KNa), KNa<sub>5</sub>MnFe<sub>13</sub>Al(PO<sub>4</sub>)<sub>11</sub>(PO<sub>3</sub>OH)(OH)<sub>2</sub>, a new arrojadite-group mineral from the Palermo No. 1 mine, New Hampshire, USA

2020· article· en· W3098977393 on OpenAlex
Inna S. Lykova, Ralph Rowe, Glenn Poirier, Kate Helwig, Henrik Friis

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueMineralogical Magazine · 2020
Typearticle
Languageen
FieldMaterials Science
TopicCrystal Structures and Properties
Canadian institutionsCanadian Museum of Nature
Fundersnot available
KeywordsMohs scale of mineral hardnessCrystallographyCrystal structureOctahedronChemistryInfrared spectroscopyMineralogyAnalytical Chemistry (journal)Materials science

Abstract

fetched live from OpenAlex

Abstract A new arrojadite-group mineral manganoarrojadite-(KNa), ideally KNa 5 MnFe 13 Al(PO 4 ) 11 (PO 3 OH)(OH) 2 , was found in a phosphate-bearing granite pegmatite at the Palermo No. 1 mine, New Hampshire, USA. It forms anhedral grains up to 1 × 1.5 cm in size combined in aggregates with vivianite, goyazite, quartz and calcite. The mineral is olive green with a pale green streak and vitreous to greasy lustre. The cleavage is good in one direction. The Mohs hardness is 4½. D calc is 3.53 g/cm 3 . Manganoarrojadite-(KNa) is optically biaxial (–), α = 1.658(2), β = 1.666(2), γ = 1.670(2), 2V meas. = 67(1)° and 2V calc. = 70° (589 nm). The infrared spectrum is reported. The composition (wt.%) is Na 2 O 6.97, K 2 O 1.78, CaO 0.31, MgO 2.17, MnO 12.30, FeO 31.17, Al 2 O 3 2.43, P 2 O 5 40.48, F 0.30, H 2 O 1.32, O = F 2 –0.13, total 99.10. The empirical formula calculated on the basis of 12 P and (O+OH+F) = 50 apfu is Na 4.73 K 0.80 Ca 0.12 Mg 1.13 Mn 2+ 3.65 Fe 2+ 9.13 Al 1.00 P 12.00 O 46.59 OH 3.08 F 0.33 . The ideal structural formula is A 1 K A 2 Na B 1 Na B 2 Na Na1,2 Na 2 Na3 □ C Mn M Fe 13 Al(PO 4 ) 11 (PO 3 OH) W (OH) 2 . The mineral is monoclinic, Cc , a = 16.5345(3), b = 10.0406(2), c = 24.6261(5) Å, β = 105.891(2)°, V = 3932.09(14) Å 3 and Z = 4. The strongest reflections of the powder X-ray diffraction pattern [ d ,Å( I )( hkl )] are: 5.902(24)(202), 5.025(24)(020), 3.208(47)(206, $\;\bar{1}$ 32), 3.048(100)( $\bar{5}$ 14, $\bar{4}$ 24), 2.758(24)( $\bar{6}$ 02) and 2.704(70)(226). The crystal structure, refined from single-crystal X-ray diffraction data ( R 1 = 0.025), is of the arrojadite structure type. Manganoarrojadite-(KNa) is the first arrojadite-group mineral with Mn dominant on the site usually occupied by Ca and without Ca as the dominant cation at any cation site.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.003
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies, Scholarly communication, Open science, Research integrity, Insufficient payload (model declined to judge)
Consensus categoriesMeta-epidemiology (narrow), Research integrity, Insufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.152
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.003
Meta-epidemiology (narrow)0.0060.004
Meta-epidemiology (broad)0.0050.003
Bibliometrics0.0010.004
Science and technology studies0.0020.003
Scholarly communication0.0030.003
Open science0.0050.003
Research integrity0.0030.004
Insufficient payload (model declined to judge)0.0010.009

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.024
GPT teacher head0.216
Teacher spread0.192 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it