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Record W3107108349 · doi:10.1002/marc.202000553

A Boron Difluoride Hydrazone (BODIHY) Polymer Exhibits Aggregation‐Induced Emission

2020· article· en· W3107108349 on OpenAlexafffund
Daniela Cappello, Alexander E. R. Watson, Joe B. Gilroy

Bibliographic record

VenueMacromolecular Rapid Communications · 2020
Typearticle
Languageen
FieldMaterials Science
TopicLuminescence and Fluorescent Materials
Canadian institutionsWestern University
FundersNatural Sciences and Engineering Research Council of CanadaOntario Ministry of Research, Innovation and Science
KeywordsMonomerPolymerPolymerizationMaterials scienceHydrazonePolymer chemistryPhotochemistryEthylene glycolAggregation-induced emissionChemical engineeringChemistryFluorescenceOrganic chemistryComposite materialOptics

Abstract

fetched live from OpenAlex

Abstract Polymers that exhibit aggregation‐induced emission (AIE) find use, for example, as cell‐imaging agents and as fluorometric sensors due to their unique optical properties. However, the structural diversity of AIE‐active polymers has not necessarily advanced at the same rate as their applications. In this work, ring‐opening metathesis polymerization is used to synthesize the first example of a polymer (Mn = 61,600 g mol−1, Đ = 1.32) containing boron difluoride hydrazone (BODIHY) heterocycles in its repeating unit. The BODIHY monomer and polymer described absorb and emit in the visible region in solution (λabs = 428 and 429 nm, λem = 528 and 526 nm) and as thin films (λabs = 443 and 440 nm, λem = 535 and 534 nm). Monomer (ΦFilm = 10%) and polymer (ΦFilm = 6%) exhibit enhanced emission as thin films compared to solution (ΦSoln ≤ 1%) as well as AIE upon the addition of water to DMF solutions as a result of restriction of intramolecular motion. Enhancement factors for the monomer and polymer are determined to be 58 and 15, respectively. The title BODIHY polymer exhibited an earlier onset of AIE and enhanced sensitivity to solution viscosity when compared to the parent monomer.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.037
GPT teacher head0.265
Teacher spread0.228 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations24
Published2020
Admission routes2
Has abstractyes

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Same venueMacromolecular Rapid CommunicationsSame topicLuminescence and Fluorescent MaterialsFrench-language works237,207