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Record W3125188928 · doi:10.1002/cjce.24035

Optimal conditions determination for hydrodeoxygenation of free fatty acids to obtain green diesel

2021· article· en· W3125188928 on OpenAlexvenueno aff
Fernando J. Durán‐Pérez, Gregorio E. Zamora, Ana K. Medina Mendoza, M. González-Brambila, Carlos Tapia, J.A. Colín-Luna, J.C. García-Martínez

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2021
Typearticle
Languageen
FieldEngineering
TopicCatalysis and Hydrodesulfurization Studies
Canadian institutionsnot available
Fundersnot available
KeywordsHydrodeoxygenationDecarbonylationChemistryHeptadecaneFugacityGibbs free energyThermodynamicsDecarboxylationOctadecaneUNIQUACOrganic chemistryNon-random two-liquid modelActivity coefficientPhysical chemistryCatalysis

Abstract

fetched live from OpenAlex

Abstract In this work, the production of green diesel involving the hydrodeoxygenation reaction of vegetable oil, such as oleic acid, producing CO or CO 2 as byproducts, was studied. This reaction takes place under hydrogen saturation to produce stearic acid; subsequently, heptadecane is produced by the decarbonylation and decarboxylation pathways, while octadecane is obtained by the subsequent hydrodeoxygenation of octadecanal. In the formation of octadecane, water is obtained as a byproduct, while the production of heptadecane leads to CO and CO 2 as byproducts of the decarbonylation and decarboxylation reactions. When considering the products and reaction routes in the hydrotreatment of triglycerides and free acids, a mathematical model was found to be reliable in determining the minimization of the Gibbs free energy of reaction over a range of reaction temperatures and pressures. This model followed the methods of Marrero‐Gani, Joback‐Reid, and Chen‐Dinivahi‐Jeng for the estimation of thermodynamic properties of the pure components. The fugacity was calculated by considering the partial fugacity coefficients, and the Peng‐Robinson equation of state and the van der Waals mixing rule were used. The mole fractions at equilibrium were estimated by least squares analysis, using MATLAB, in order to account for non‐idealities in reaction thermodynamic properties and to find the equilibrium composition that minimized the total Gibbs free energy. Likewise, the reaction coordinates of the equilibrium reaction were estimated together with the known values of the composition in order to know the effect of pressure and temperature on the aforementioned reactions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.404
Threshold uncertainty score0.324

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.213
Teacher spread0.202 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2021
Admission routes1
Has abstractyes

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