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Record W3134393763 · doi:10.1021/acsomega.0c05815

Hexachlorocyclotriphosphazene Functionalized Graphene Oxide as a Highly Efficient Flame Retardant

2021· article· en· W3134393763 on OpenAlexafffund
Khaled Rhili, Siham Chergui, Ahmad Samih ElDouhaibi, Mohamed Siaj

Bibliographic record

VenueACS Omega · 2021
Typearticle
Languageen
FieldMaterials Science
TopicFlame retardant materials and properties
Canadian institutionsUniversité du Québec à Montréal
FundersFonds Québécois de la Recherche sur la Nature et les TechnologiesNatural Sciences and Engineering Research Council of CanadaCanada Research ChairsCanada Foundation for Innovation
KeywordsThermogravimetric analysisFire retardantMaterials scienceDiglycidyl etherThermal stabilityThermosetting polymerEpoxyGrapheneFourier transform infrared spectroscopyOxideChemical engineeringComposite materialRaman spectroscopyPolymer chemistryBisphenol ANanotechnologyMetallurgy

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide A flame-retardant composite was synthesized through a simple graphene oxide functionalization route with hexachlorocyclotriphosphazene and p -phenylenediamine. Flame experiments conducted on the synthesized composite proved its importance as tremendously resistant to fire. The thermogravimetric analysis (TGA) shows clearly that the functionalized graphene oxide (FGO) exhibits an enhanced thermal stability and better temperature resistance. A thermoset epoxy resin was prepared by incorporating different percentages (2, 5, and 10%) of FGO to diglycidyl ether of bisphenol A (DGEBA). The flame-retardant properties, thermal degradation behavior, and combustion of the DGEBA thermosets cured by m -phenylenediamine were investigated using a Bunsen burner flame approaching the flame temperature of a fire and TGA. The chemical structure of FGO was characterized with spectroscopic and imaging techniques including Fourier transform infrared spectroscopy, Raman spectroscopy, X-ray diffraction, TGA, scanning electron microscopy, energy-dispersive X-ray spectroscopy elemental mapping, and X-ray photoelectron spectroscopy. Due to its high flame-retardant capabilities, such a composite could promise potential applications in the manufacture of inflammable materials for different uses.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.001

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.220
Teacher spread0.207 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations37
Published2021
Admission routes2
Has abstractyes

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Same venueACS OmegaSame topicFlame retardant materials and propertiesFrench-language works237,207