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Record W31560363 · doi:10.1039/c9dt03143j

MÉTODE ROLE PLAYING PIKEUN NGARONJATKEUN KAMAMPUH NYARITA NGAGUNAKEUN TATAKRAMA BASA SUNDA (STUDI KUASI ÉKSPÉRIMÉN KA SISWA KELAS VIIA SMP YAS BANDUNG TAUN AJARAN 2013/2014)

2014· article· en· W31560363 on OpenAlex
Dely Nurma Antari

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

fundA Canadian funder is recorded on the work.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldComputer Science
TopicEducational Methods and Media Use
Canadian institutionsnot available
FundersCanadian Network for Research and Innovation in Machining Technology, Natural Sciences and Engineering Research Council of CanadaCompute Canada
KeywordsHumanitiesPsychologyArt

Abstract

fetched live from OpenAlex

This work investigates the hydrogenation of carbon dioxide to formate catalysed by the phosphine-free Ru complexes Ru(OtBu)(κ<sup>3</sup>-NCN)(<sup>tBu</sup>bpy) and RuH(OtBu)(κ<sup>2</sup>-NCN)(<sup>tBu</sup>bpy) (OtBu = tert-butoxide, κ<sup>2</sup>-NCN = 1,3-di(2-methylpyridyl)-4,5-diphenyl-1H-imidazol-2-ylidene, where one pyridyl moiety is not coordinated to Ru, <sup>tBu</sup>bpy = 4,4'-di-tert-butyl-2,2'-dipyridyl). A catalytic cycle is proposed for this reaction, supported by computational studies and the characterization of the hydride and the formate intermediates proposed to be involved. Modest catalytic turnovers are demonstrated at relatively low pressures and temperatures. The proposed rate determining step is heterolytic H<sub>2</sub> splitting to regenerate the Ru-H complex, which has an estimated hydricity of approx. 27 kcal mol<sup>-1</sup>. The κ<sup>2</sup>-NCN ligand in the hydride complex undergoes a variety of dynamic processes as detected by EXSY spectroscopy including a pyridyl "roll-over" carbon-hydrogen - ruthenium hydride exchange, possibly occuring via a Perutz-Sabo-Etienne CAM mechanism.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: none
GenreCandidate signal: Methods · Consensus signal: Methods
Teacher disagreement score0.584
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0030.001
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0010.000
Scholarly communication0.0010.001
Open science0.0030.001
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.271
Teacher spread0.255 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Quick stats

Citations0
Published2014
Admission routes1
Has abstractyes

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