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Record W3156138561 · doi:10.1021/jacs.1c00384

Stabilizing Highly Active Ru Sites by Suppressing Lattice Oxygen Participation in Acidic Water Oxidation

2021· article· en· W3156138561 on OpenAlexafffund
Yunzhou Wen, Peining Chen, Lu Wang, Shangyu Li, Ziyun Wang, Jehad Abed, Xinnan Mao, Yimeng Min, Cao‐Thang Dinh, Phil De Luna, Rui Huang, Longsheng Zhang, Lie Wang, Liping Wang, Robert J. Nielsen, Huihui Li, Tao‐Tao Zhuang, Changchun Ke, Oleksandr Voznyy, Yongfeng Hu, Youyong Li, William A. Goddard, Bo Zhang, Huisheng Peng, Edward H. Sargent

Bibliographic record

VenueJournal of the American Chemical Society · 2021
Typearticle
Languageen
FieldEnergy
TopicElectrocatalysts for Energy Conversion
Canadian institutionsCanadian Light Source (Canada)Queen's UniversityCanada Research ChairsUniversity of Toronto
FundersDivision of Chemical, Bioengineering, Environmental, and Transport SystemsBeijing Synchrotron Radiation FacilityNatural Sciences and Engineering Research Council of CanadaOffice of ScienceMinistry of Science and Technology of the People's Republic of ChinaNorthwestern Polytechnical UniversityU.S. Department of EnergyCalifornia Institute of TechnologySalt Science Research FoundationCanadian Institute for Advanced ResearchE-Institutes of Shanghai Municipal Education CommissionShanghai Municipal Education CommissionNational Natural Science Foundation of ChinaNorthwestern UniversityScience and Technology Commission of Shanghai MunicipalityNational Science Foundation
KeywordsChemistryOverpotentialOxygen evolutionWater splittingCatalysisInorganic chemistryElectrolyteElectrochemistryPhysical chemistryElectrodePhotocatalysis

Abstract

fetched live from OpenAlex

In hydrogen production, the anodic oxygen evolution reaction (OER) limits the energy conversion efficiency and also impacts stability in proton-exchange membrane water electrolyzers. Widely used Ir-based catalysts suffer from insufficient activity, while more active Ru-based catalysts tend to dissolve under OER conditions. This has been associated with the participation of lattice oxygen (lattice oxygen oxidation mechanism (LOM)), which may lead to the collapse of the crystal structure and accelerate the leaching of active Ru species, leading to low operating stability. Here we develop Sr–Ru–Ir ternary oxide electrocatalysts that achieve high OER activity and stability in acidic electrolyte. The catalysts achieve an overpotential of 190 mV at 10 mA cm –2 and the overpotential remains below 225 mV following 1,500 h of operation. X-ray absorption spectroscopy and 18 O isotope-labeled online mass spectroscopy studies reveal that the participation of lattice oxygen during OER was suppressed by interactions in the Ru–O–Ir local structure, offering a picture of how stability was improved. The electronic structure of active Ru sites was modulated by Sr and Ir, optimizing the binding energetics of OER oxo-intermediates.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.254
Teacher spread0.244 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations548
Published2021
Admission routes2
Has abstractyes

Explore more

Same venueJournal of the American Chemical SocietySame topicElectrocatalysts for Energy ConversionFrench-language works237,207