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Record W3164264121 · doi:10.1002/9783527825028.ch12

Biomass Processing via Mechanochemical Means

2021· other· en· W3164264121 on OpenAlexaff
Georgios Margoutidis, Francesca M. Kerton

Bibliographic record

Venuenot available
Typeother
Languageen
FieldMaterials Science
TopicAdvanced Cellulose Research Studies
Canadian institutionsMemorial University of Newfoundland
Fundersnot available
KeywordsMechanochemistryCelluloseBall millChitinDepolymerizationExtrusionChemical engineeringBiomass (ecology)Materials sciencePulp and paper industryLigninYield (engineering)BiofuelOrganic chemistryChemistryChitosanWaste managementComposite materialEngineering

Abstract

fetched live from OpenAlex

Mechanochemistry can be performed on a wide range of biomass feedstocks using mixer/shaker mills, planetary mills, or extrusion devices. Using a mechanochemical approach to transform renewable feedstocks can lead to significant reductions in solvent and energy use. A brief description of how mechanochemistry works on a molecular level is provided, and further details on a typical mixer mill system are presented. In developing a mechanochemical process, chemical (e.g. type of reaction), technological (e.g. milling material), and process (e.g. frequency of milling) parameters must be taken into account and optimized on a case-by-case basis. Examples of where mechanochemistry has been successfully applied to depolymerization of cellulose, chitin, and lignin are described. Amorphization of chitin and cellulose through grinding can allow new chemistries to be accessed, which are not possible in the solution phase. Modification of cellulose to yield a thermoplastic and deacetylation of chitin to form chitosan has also been successful. Potentially bio-sourced small molecules, such as amino acids and nucleotides, have also been transformed under mechanochemical conditions including the solvent-free production of the sweetener aspartame. Mechanochemistry has been applied to a limited extent to biominerals. The varied range of chemistries and feedstocks that can be transformed through milling or extrusion will lead to continued research in this area.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Other · Consensus signal: Other
Teacher disagreement score0.215
Threshold uncertainty score0.977

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0240.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.026
GPT teacher head0.313
Teacher spread0.287 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreOther

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations12
Published2021
Admission routes1
Has abstractyes

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Same topicAdvanced Cellulose Research StudiesFrench-language works237,207