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Record W3175962317 · doi:10.1016/j.jcat.2021.06.020

New insights on CO and CO2 hydrogenation for methanol synthesis: The key role of adsorbate-adsorbate interactions on Cu and the highly active MgO-Cu interface

2021· article· en· W3175962317 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

fundA Canadian funder is recorded on the work.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueJournal of Catalysis · 2021
Typearticle
Languageen
FieldChemical Engineering
TopicCatalysts for Methane Reforming
Canadian institutionsnot available
FundersHorizon 2020European Research CouncilHorizon 2020 Framework ProgrammeVillum FondenUniversity of TorontoDanmarks Tekniske UniversitetEuropean CommissionStanford University
KeywordsChemistryFormateCatalysisMethanolDensity functional theoryAdsorptionHydrogenPhotochemistryTransition metalHeterogeneous catalysisCarbon monoxideInorganic chemistryTransition stateReaction intermediateComputational chemistryPhysical chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

By coupling density functional theory calculations (DFT) with microkinetic modeling, we address two controversial problems pertaining to methanol synthesis: i) Which of the CO or CO2 hydrogenation routes dominates the synthesis rate, and ii) what makes irreducible, inert oxides like MgO an efficient promoter for the CO hydrogenation process? We determine that the inconsistency between the experimental activity trend and the previous theoretical results in the literature is attributed to the absence of interactions between adsorbed formate and intermediates, which would underestimate the rate of CO2 route by having a too high formate coverage. We show that when adsorbate-adsorbate interactions, especially the derived H bond, are included, the CO2 hydrogenation dominates for pure Cu catalysts, which is consistent with experiments. In addition, a new transition state for hydrogenation of adsorbed HCOOH* is discovered, which is further stabilized by hydrogen bonding. We also identify the MgO/Cu interface as a highly active site and propose a novel lattice-oxygen involved reaction mechanism at the interface for methanol formation. The CO hydrogenation reactivity can then be enhanced by stabilizing HCO* in the formate-type species, while the CO2 hydrogenation is inhibited by the poisoning of CO2* and HCOO*.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.036
Threshold uncertainty score0.423

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.255
Teacher spread0.245 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it