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Record W3177328136 · doi:10.1002/er.6974

Enhanced electrochemical performance of battery‐grade cobalt phosphate via magnetron sputtered copper interfacial layer for potential supercapattery applications

2021· article· en· W3177328136 on OpenAlexaff
Muhammad Zahir Iqbal, Junaid Khan, S. Alam, Rashid Ali, Amir Muhammad Afzal, Sikandar Aftab

Bibliographic record

VenueInternational Journal of Energy Research · 2021
Typearticle
Languageen
FieldMaterials Science
TopicSupercapacitor Materials and Fabrication
Canadian institutionsSimon Fraser University
Fundersnot available
KeywordsMaterials scienceCopperCobaltScanning electron microscopeNickelElectrodeSputter depositionElectrochemistryCavity magnetronLayer (electronics)Chemical engineeringMetallurgyComposite materialNanotechnologySputteringThin filmChemistry

Abstract

fetched live from OpenAlex

The supercapattery has achieved significant prominence for its high specific energy and power: however, still craved for electrodes with high ionic conduction and superior electrochemical performance. The study demonstrates the tuned electrochemical performance of cobalt phosphate via introducing a magnetron sputtered copper interfacial layer. Cobalt phosphate nanomaterials synthesized via the sonochemical approach was utilized as active electrode material. The magnetron sputter technique was employed to deposit copper on current collector (nickel foam). The structural studies and morphological aspects and elemental analysis were analyzed via X-ray diffraction, scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy. Atomic force microscopy (AFM) was performed to scrutinize the surface morphology of magnetron sputtered copper. The cobalt phosphate deposited on copper sputtered nickel foam profits a specific capacity (Qs) of 403.1 C/g (120.9% as compared to bare nickel foam) at 3 mV/s and 348.4 C/g (135.7% as compared with bare nickel foam) at 0.6 A/g in three electrode assembly. This electrode was further utilized in an asymmetric architecture (supercapattery device) that delivers outstanding Qs of 265.2 C/g with excellent Es of 62.6 Wh/kg and Ps of 425 W/kh at 0.5 A/g. The device also delivers an excellent Ps of 7924 W/kg while retaining Es of 11.8 Wh/kg at 7 A/g. Moreover, outstanding capacitive retention of 92.9% was observed after 5000 consecutive charge discharge cycles. In addition, the hybrid performance of the designed supercapattery was also explored via a theoretical methodology. The maximum diffusive and capacitive contribution of 88.81% (at 3 mV/s) and 55.11% (at 100 mV/s) was grasped by the device. To the best of our knowledge, this is the first approach toward the utilization of magnetron sputtered interfacial nanograins layer to tune the electrochemical performance of electrode material for potential supercapattery devices.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.052
Threshold uncertainty score0.955

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.032
GPT teacher head0.323
Teacher spread0.291 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations22
Published2021
Admission routes1
Has abstractyes

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