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Record W3193797780 · doi:10.1109/lsens.2021.3103433

Molecularly Imprinted Electroimpedance Sensor for Detection of 8-Isoprostane in Exhaled Breath Condensate

2021· article· en· W3193797780 on OpenAlexafffund
Bruno Gamero, Siziwe Bebe, Ravi Prakash

Bibliographic record

VenueIEEE Sensors Letters · 2021
Typearticle
Languageen
FieldChemistry
TopicAnalytical chemistry methods development
Canadian institutionsCarleton University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsMolecularly imprinted polymerAnalyteExhaled breath condensateChemistryBiomarkerBreath gas analysisBiomoleculeExhaled airPolymerChromatographyBiochemistryOrganic chemistrySelectivityMedicineInternal medicine

Abstract

fetched live from OpenAlex

Soft lithographically patterned molecularly imprinted polymers (MIP) offer highly durable, low-cost fabricated biochemical sensors, with a highly selective biorecognition mechanism. In MIP architecture, nanocavity binding sites are imprinted onto a polymer thin film coated over an interdigitated electrode structure. As the target molecules affixed to the binding sites, the frequency-dependent electroimpedance is measured across the interdigitated electrode, and the response signal is analyzed to determine analyte concentration. This letter uses poly(vinyl alcohol), N-methyl-4 (4'-formylstyryl)pyridinium methosulfate acetal (PVA-SbQ) to create the desired MIP thin film structure for detecting specific physiologically relevant small molecules, 8-isoprostane, and an oxidative stress biomarker clinical tested in blood or saliva samples. The sensor devices were rigorously tested against comparable biomolecules, including cortisol, cortisone, and progesterone, demonstrating very minimal cross sensitivity, mostly at very high concentrations and well above their physiological concentration range in exhaled breath condensate. The detectable range of 8-isoprostane in aerosolized test and control samples mimicking exhaled breath condensate was identified as 1-100 pg/mL, which comfortably covers the reported physiological concentration range (10-100 pg/mL) of this biomarker in exhaled breath.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.263
Teacher spread0.248 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations8
Published2021
Admission routes2
Has abstractyes

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Same venueIEEE Sensors LettersSame topicAnalytical chemistry methods developmentFrench-language works237,207