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Record W3206036601 · doi:10.1021/acs.jpcc.1c06627

An Effective Medium Theory Description of Surface-Enhanced Infrared Absorption from Metal Island Layers Grown on Conductive Metal Oxide Films

2021· article· en· W3206036601 on OpenAlexafffund
Ian R. Andvaag, Erick Lins, Ian J. Burgess

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2021
Typearticle
Languageen
FieldMaterials Science
TopicGold and Silver Nanoparticles Synthesis and Applications
Canadian institutionsUniversity of Saskatchewan
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsMaterials scienceOxideIndium tin oxideElectric fieldAbsorption (acoustics)DielectricAnalytical Chemistry (journal)Thin filmOpticsCondensed matter physicsOptoelectronicsChemistryComposite materialNanotechnology

Abstract

fetched live from OpenAlex

The influence of a thin film of a supporting layer of conductive metal oxide (CMO) on the surface-enhanced infrared spectra generated from metal island layers is studied using an effective medium (EM) approximation and compared to experimental results. Gold island films electrodeposited on indium tin oxide (ITO) coated on an internal reflection element (IRE) give rise to asymmetric (bimodal or derivative-looking) line shapes and have strong surface-enhanced infrared absorption spectroscopy (SEIRAS) intensities for adsorbed cyanate using both p- (transverse magnetic) and s- (transverse electric) plane-polarized light. The dependence of the SEIRAS intensity on the angle of incidence is very different compared to metal films directly deposited on the surface of the IRE, as larger magnitude SEIRAS intensities are observed at angles close to the critical angle. The role of additional enhancement effects from possible plasmonic phenomena arising in the ITO layer is shown not to contribute to the ATR-SEIRAS mechanism. The observed spectra are modeled using an EM treatment of the gold island film, and a good qualitative and semiquantitative agreement is found between the calculated and experimental results. Using the Fresnel equations and EM-determined optical constants, the reflectivity of the interface is shown to be highly dependent on the volume fraction of gold in the enhancing layer, and asymmetric and even inverted bands arise near the metal percolation threshold. Electric field analysis shows that the low free charge carrier density (relative to metals) of ITO gives rise to field distributions similar to those of an absorbing dielectric layer on the surface of an IRE.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.003
Threshold uncertainty score0.009

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0010.000
Science and technology studies0.0000.001
Scholarly communication0.0010.001
Open science0.0020.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0030.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.241
Teacher spread0.229 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations22
Published2021
Admission routes2
Has abstractyes

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Same venueThe Journal of Physical Chemistry CSame topicGold and Silver Nanoparticles Synthesis and ApplicationsFrench-language works237,207