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Record W3207745777 · doi:10.1117/12.2601143

Simplified gluten detection approach in the presence of a black hole quencher (BHQ)

2021· article· en· W3207745777 on OpenAlexaff
Samaria Nevarez Diaz, Orly Yadid-Pecht, Varun Vij, Raymond J. Turner

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicAdvanced biosensing and bioanalysis techniques
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsFörster resonance energy transferFluorophoreBiosensorConjugateCovalent bondChemistryFluorescenceGliadinConjugated systemReagentCombinatorial chemistryQuenching (fluorescence)GrapheneFluoresceinGlutenChromatographyNanotechnologyMaterials scienceOrganic chemistryBiochemistryPolymer

Abstract

fetched live from OpenAlex

Optical biosensors based in the fluorescence resonance energy transfer (FRET) phenomenon require of fluorophores. The use of fluorophores requires of a complex optical system that often leads to signal loss. Thus, a new approach based in a Black Hole Quencher (BHQ) that further simplifies the biosensor is sought. This approach potentially increases the sensitivity and accuracy. For the development of this approach, the gliadin conjugate with BHQ-10 must be established first. In the present work, we used the physical phenomenon of FRET to study the gliadin conjugation with BHQ-10 molecule. We performed an experiment with a fluorophore (6-Carboxyfluorescein or 6-FAM) labeled aptamer and non-covalently attached to graphene oxide (GO). The gliadin from gluten was conjugated with BHQ using two different cross-linking reagents present in BHQ: BHQ-10 succinimidyl ester and BHQ-10 carboxylic acid. BHQ-10 with carboxylic acid as the cross-linking reagent demonstrated to be an efficient reaction for gliadin conjugation with BHQ-10. The average quenching efficiency obtained was 62% in comparison to the gliadin as a control experiment. This sets the basis for the breakthrough development of a simplified gluten detection biosensor based on absorbance measurements instead of different wavelength ranges as fluorophores do. The aim is to develop a point-of-care microfluidic system that measures gliadin from gluten in a sensitive, accurate and cost-efficient manner.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.269
Teacher spread0.255 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2021
Admission routes1
Has abstractyes

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