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Record W4210313577 · doi:10.46770/as.2022.008

Scanning Transmission X-Ray Microscopy At The Canadian Light Source: Progress And Selected Applications In Geosciences

2022· article· en· W4210313577 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.
aboutThe title or abstract carries a Canadian signal from the geographic lexicon.

Bibliographic record

VenueAtomic Spectroscopy · 2022
Typearticle
Languageen
FieldEngineering
TopicAdvanced X-ray and CT Imaging
Canadian institutionsCanadian Light Source (Canada)University of Saskatchewan
FundersNatural Sciences and Engineering Research Council of CanadaInstitute of Geology and Geophysics, Chinese Academy of SciencesCanadian Institutes of Health ResearchNational Natural Science Foundation of ChinaChinese Academy of SciencesUniversity of SaskatchewanCanadian Light Source
KeywordsChemistryMicroscopyX-rayOpticsAnalytical Chemistry (journal)NanotechnologyEnvironmental chemistryPhysicsMaterials science

Abstract

fetched live from OpenAlex

Synchrotron-based scanning transmission X-ray microscopy (STXM) efficiently integrates X-ray microscopy and X-ray absorption spectroscopy (XAS) to provide quantitative, chemically specific imaging of elements, functional groups, bonding, and oxidation states in 2D and 3D modes at high spatial resolution (sub-10 to 30 nm), high energy resolution, and low radiation doses. STXM has been increasingly used to study various materials and samples for life, earth, planetary, and environmental sciences. In this progress report and minireview, the STXM principle and instrumentation of conventional STXM and the latest STXM-ptychography at the Canadian Light Source are first discussed. Then, two representative applications of STXM on geoscience-related samples, including magnetotactic bacteria, soil microaggregates, and related systems, are presented to illustrate the strong capabilities and suitability of STXM to elucidate complex systems, processes, and associations in the natural sciences. Finally, the potential applications and prospects of the STXM-related techniques in characterizing precious extraterrestrial samples (e.g., lunar samples returned by China's Chang'e-5 mission) are briefly discussed.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.507
Threshold uncertainty score0.840

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0010.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.003
GPT teacher head0.224
Teacher spread0.220 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it