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Record W4226449825 · doi:10.3389/fmats.2022.839421

Conversion of Waste Corn Biomass to Activated Bio-Char for Applications in Wastewater Treatment

2022· article· en· W4226449825 on OpenAlexaff
Shokooh Karami, Sadegh Papari, Franco Berruti

Bibliographic record

VenueFrontiers in Materials · 2022
Typearticle
Languageen
FieldEnvironmental Science
TopicAdsorption and biosorption for pollutant removal
Canadian institutionsWestern University
Fundersnot available
KeywordsCharActivated carbonBET theoryPyrolysisSpecific surface areaBiocharChemistryAdsorptionActivated sludgeNuclear chemistryChemical engineeringMaterials scienceWastewaterCatalysisWaste managementOrganic chemistry

Abstract

fetched live from OpenAlex

This study proposes the conversion of waste corn grains contaminated by deoxynivalenol (also known as vomitoxin), a mycotoxin produced by plant pathogens, into a value-added product. Batches of 500 g of contaminated corn grains were pyrolyzed in a batch reactor by thermal treatment at temperatures up to 500°C with a 15°C/min heating rate and generating condensable vapors, gases and solid bio-char. The bio-char produced was subsequently activated in a furnace at 900°C, using CO2 as an activation agent, at different residence times. The effect of activation residence time on the characteristics of the activated bio-char, varying it from 0.5 to 3 h, was investigated. Characterization tests included BET surface area, SEM, TG-FTIR, pH, and XRD on both bio-char and activated bio-char. BET results illustrated a significant increase of the surface area from 63 to 419 m2g−1 and pore volume from 0.04 to 0.23 cm3g−1 by increasing the activation time from 0.5 to 3 h. SEM images visually confirmed a considerable increase in pore development. The pH significantly increased from 6 to 10 after activation, due to the elimination of acidic functional groups. The proximate analysis showed the stable carbon of the activated char reaching approximately 90 wt%, making it promising for catalyst/adsorbent applications. The adsorption performance of activated bio-char was tested by utilizing three different model molecules with different characteristics: methylene blue, methyl orange, and ibuprofen. Among all activated bio-char samples, activated bio-char with 3 h activation time showed the highest adsorption capacity, with a total adsorption (25 mg/g of activated bio-char) of methylene blue after 5 min. The results showed that the adsorption capacity of the activated bio-char was similar to that of valuable commercial activated carbon.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.228
Teacher spread0.217 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations14
Published2022
Admission routes1
Has abstractyes

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