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Record W4229003552 · doi:10.26434/chemrxiv-2022-k2snf

Coupled interfacial and bulk kinetics govern the timescales of multiphase ozonolysis reactions

2022· preprint· en· W4229003552 on OpenAlexfundno aff
Megan D. Willis, Kevin R. Wilson

Bibliographic record

VenueChemRxiv · 2022
Typepreprint
Languageen
FieldEarth and Planetary Sciences
TopicAtmospheric chemistry and aerosols
Canadian institutionsnot available
FundersLawrence Berkeley National LaboratoryChemical Sciences, Geosciences, and Biosciences DivisionNatural Sciences and Engineering Research Council of CanadaBasic Energy SciencesUniversity of BristolRoyal Holloway, University of LondonU.S. Department of Energy
KeywordsOzonolysisAerosolChemistryDiffusionParticle (ecology)Kinetic energyChemical physicsThermodynamicsOzoneReaction rateKineticsAqueous solutionPhysical chemistryOrganic chemistryPhysics

Abstract

fetched live from OpenAlex

Chemical transformations in aerosol impact the lifetime of particle-phase species, the fate of atmospheric pollutants, and both climate and health-relevant aerosol properties. Timescales for multiphase reactions of ozone in atmospheric aqueous phases are governed by coupled kinetic processes between the gas-phase, the particle interface and its bulk, which respond dynamically to reactive consumption of O3. However, models of atmospheric aerosol reactivity often do not account for the coupled nature of multiphase processes. To examine these dynamics, we use new and prior experimental observations of aqueous droplet reaction kinetics, including three systems with a range of surface affinities and ozonolysis rate coefficients (trans-aconitic acid (C6H6O6), maleic acid (C4H4O4) and sodium nitrite (NaNO2)). Using literature rate coefficients and thermodynamic properties, we constrain a simple two-compartment stochastic kinetic model, which resolves the interface from the particle bulk and represents O3 partitioning, diffusion and reaction as a coupled kinetic system. Our kinetic model accurately predicts decay kinetics across all three systems, demonstrating that both the thermodynamic properties of O3 and the coupled kinetic and diffusion processes are key to making accurate predictions. An enhanced concentration of adsorbed O3, compared to gas and bulk phases, is rapidly maintained and remains constant even as O3 is consumed by reaction. Multiphase systems dynamically seek to achieve equilibrium in response to reactive O3 loss, but this is hampered at solute concentrations relevant to aqueous aerosol by the rate of O3 arrival in the bulk by diffusion. As a result, bulk-phase O3 becomes depleted from its Henry’s Law solubility. This bulk-phase O3 depletion limits reaction timescales for relatively slow-reacting organic solutes with low interfacial affinity (i.e., trans-aconitic and maleic acids, with krxn ~ 10^3 - 104 M-1 s-1), which is in contrast to fast-reacting solutes with higher surface affinity (i.e., nitrite, with krxn ~ 10^5 M-1 s-1) where surface reactions strongly impact observed decay kinetics.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.002
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.012

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.002
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0010.002
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.229
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations7
Published2022
Admission routes1
Has abstractyes

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