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Record W4231702042 · doi:10.1520/mnl12251m

Chromatography

2012· book-chapter· en· W4231702042 on OpenAlexaff
Rolando C. Domingo, Rey G. Montemayor

Bibliographic record

Venuenot available
Typebook-chapter
Languageen
FieldChemistry
TopicAnalytical Chemistry and Chromatography
Canadian institutionsImperial Oil (Canada)
Fundersnot available
KeywordsChromatographyChemistry

Abstract

fetched live from OpenAlex

CHROMATOGRAPHY IS A TERM THAT DENOTES A myriad of laboratory separation processes based on a differential migration phenomenon. It is particularly effective for the resolution and separation of complex mixtures; hence, it can be used as a chemical preparatory method or, more importantly, as an analytical tool. This potent analytical technique has been widely used in the paint industry for a broad range of coating applications from everyday routine analysis to fundamental research into the nature of organic coating systems. Its use has been so extensive that virtually every type of material used in paint has been affected by chromatography. Chromatography possesses certain inherent features that offer distinct advantages over conventional analytical techniques: complex mixtures, including isomers and homologs, can be separated; most of the equipment is relatively simple and inexpensive; chromatographic procedures are applicable to a broad spectrum of chemical types and are adaptable to both micro- and macro-size samples; and chromatography is capable of both qualitative and quantitative functions even when applied to multicomponent systems. The term chromatography was coined by Tswett [1] who, in 1906, used powdered chalk and petroleum ether to separate plant pigments into colored zones of isolated pigment. The technique, as described by Tswett was largely ignored for a long time, and it was not until the late 1930s and early 1940s that Martin and Synge [2] applied the technique successfully to colorless materials, but the name has persisted. The term is currently used to signify a broad group of separation techniques, most of which are independent of color.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.006
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: Not applicable
GenreCandidate signal: Other · Consensus signal: Other
Teacher disagreement score0.209
Threshold uncertainty score0.700

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0030.006
Meta-epidemiology (narrow)0.0030.001
Meta-epidemiology (broad)0.0040.002
Bibliometrics0.0060.004
Science and technology studies0.0040.002
Scholarly communication0.0050.004
Open science0.0050.005
Research integrity0.0030.005
Insufficient payload (model declined to judge)0.2090.248

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.210
Teacher spread0.197 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designNot applicable
Domainnot available
GenreOther

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2012
Admission routes1
Has abstractyes

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