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Record W4238005813 · doi:10.1021/ie060524t

Formation and Characteristics of Carbonaceous Deposits from Heavy Hydrocarbon Coking Vapors

2006· article· en· W4238005813 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2006
Typearticle
Languageen
FieldEngineering
TopicCyclone Separators and Fluid Dynamics
Canadian institutionsUniversity of British Columbia
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsCoker unitThermogravimetric analysisElemental analysisAsphaltCondensationFoulingScanning electron microscopeDeposition (geology)Chemical engineeringCharacterization (materials science)ChemistryHydrocarbonDistillationtar (computing)CokeMineralogyMaterials scienceGeologyNanotechnologyChromatographyMembraneOrganic chemistryComposite materialSediment

Abstract

fetched live from OpenAlex

Deposition of carbonaceous material in the cyclone exit line is a chronic problem for fluid cokers and is a key process limitation to achieving longer run length. Extensive characterization studies were conducted for laboratory deposits from a bench-scale bitumen coker using modern analytical techniques, e.g., elemental analysis, X-ray fluorescence, thermogravimetric analysis, scanning electron microscopy, diffusive reflection infrared spectroscopy, and solid-state 13 C nuclear magnetic resonance. Simulated distillation was also applied to solvent extracts of deposits. Results substantiate that on the laboratory scale physical condensation rather than chemical reaction was the primary reason for fluid coker cyclone exit line fouling. Entrained liquid droplets also contribute to the deposit formation. Although there are both polyaromatic and aliphatic structures in fresh laboratory deposits, the former dominate. High-temperature operation led to deposits an increased polyaromatic content. Industrial deposits are more cokelike than laboratory deposits, and they differ in morphology.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.341
Threshold uncertainty score0.872

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.240
Teacher spread0.219 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it