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Record W4245500033 · doi:10.1021/acs.macromol.5b01853

Amphiphilic Block Copolymers as Stabilizers in Emulsion Polymerization: Effects of the Stabilizing Block Molecular Weight Dispersity on Stabilization Performance

2015· article· en· W4245500033 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueMacromolecules · 2015
Typearticle
Languageen
FieldChemistry
TopicAdvanced Polymer Synthesis and Characterization
Canadian institutionsQueen's University
FundersBASF Corporation
KeywordsDispersityCopolymerPolymer chemistryEmulsion polymerizationMolar mass distributionStyrenePolymerizationAcrylic acidRadical polymerizationEmulsionChemistryAmphiphileZeta potentialMaterials scienceChemical engineeringOrganic chemistryPolymerNanotechnologyNanoparticle

Abstract

fetched live from OpenAlex

Molecular weight dispersity is not typically studied as a design parameter of block copolymer stabilizers but is often assumed to impact stabilization performance; low molecular weight dispersity is generally assumed to be associated with best performance. This is the first quantitative investigation of the effects of block copolymer molecular weight dispersity with regards to stabilization performance in an emulsion polymerization. Poly(styrene)- b -poly(acrylic acid) block copolymers were synthesized by nitroxide-mediated radical polymerization and employed as stabilizers in the emulsion polymerization of styrene. The effect of the stabilizing poly(acrylic acid) block molecular weight dispersity on stabilization behavior was studied, independent of molecular weight and composition. Block copolymer stabilizers were evaluated in terms of critical aggregation concentration, dispersed phase particle size, distribution, and zeta potential. The molecular weight dispersity of the stabilizing block affected the aggregation number and final number of particles but displayed no negative effects on stability or size distribution.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.026
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.212
Teacher spread0.205 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it