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Record W4246614563 · doi:10.1021/acs.jpcc.7b05803

Replacing the Al<sub>2</sub>O<sub>3</sub> Shell on Al Particles with an Oxidizing Salt, Aluminum Iodate Hexahydrate. Part I: Reactivity

2017· article· en· W4246614563 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

fundA Canadian funder is recorded on the work.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2017
Typearticle
Languageen
FieldEngineering
TopicEnergetic Materials and Combustion
Canadian institutionsnot available
FundersArmy Research OfficeAlberta Innovates - Health Solutions
KeywordsPassivationIodateOxidizing agentReactivity (psychology)AluminiumNanoparticleInorganic chemistryMaterials scienceOxygenTransmission electron microscopyChemistryIodideAnalytical Chemistry (journal)MetallurgyLayer (electronics)NanotechnologyChromatographyOrganic chemistry

Abstract

fetched live from OpenAlex

Improvements in the reactivity, measured in terms of flame speed, for aluminum-based energetic mixtures are increased by a factor of 2–3 by replacing the Al 2 O 3 passivation layer of aluminum (Al) nanoparticles with aluminum iodate hexahydrate (AIH), an oxidizing salt. The Al–AIH nanoparticles are examined under transmission electron microscopy. An AIH passivation shell surrounding the Al core particle is a more reactive composite structure than Al 2 O 3 passivation around Al which facilitates increased reaction rates with flame speeds as high as 3200 m/s. Flame speed measurements are used to show that reaction rates in AIH mixtures are determined by the AIH/Al 2 O 3 ratio, oxygen balance, and β-HIO 3 . Further optimization of these properties will ultimately boost significant increases in the reaction rates of the energetic materials presented in this article.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score0.605

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.217
Teacher spread0.206 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it